The URL can be used to link to this page

Home My WebLink About3303; Agua Hedionda Sewage Pump Station; Agua Hedionda Sewage Pump Station; 1991-07-10LEICHTON AND ASSOCIATES, INC Geotechnical and Environmental Engineering Consultants July 10, 1991 Project No. 4901121-04 To: Attention: Subject: Reference: County of San Diego Environmental Health Services Hazardous Materials Management Division P.O. Box 85261 San Diego, California 92138-5261 Mr. Mo Lahsaie Additional Requested Information Regarding Soil Sampling at the Agua Hedionda Sewage Pump Station, Carlsbad, California Leighton and Associates, Inc., 1991, Additional Verification Soil Sampling at the Aqua Hedionda Sewage Pump Station, Carlsbad, California, Project No. 4901121-04, dated June 25 In accordance with your request during our telephone conversation on July 10,1991, we are providing the additional information. 1. Question: What is the fate of the existing stockpile? Answer: It is our understanding that the City of Carlsbad intends to utilize the stockpile soil as fill material and to leave the soil stockpile in its present location (see Figure 2 of the referenced report). The stockpile will be covered with clean fill soil to prevent volatilization. It is also our understanding that the stockpile is currently covered with plastic sheeting. 2. Question: What reference was used to determine that the depth to ground water beneath the stockpiled soils is greater than 15 feet? Answer: The soil stockpile is located at the top of a cut slope 25 feet south of the pump station and at an elevation 13 feet above the pump station (see Figure 2 of the referenced report). Soil samples were collected at a depth of 3 feet below grade of the pump station. Ground water was not encountered in the excavations from which the soil samples were collected. Therefore, it was interpreted that the ground water table is greater than 15 feet below the base of the soil stockpile. In addition, seeps were not observed in the cut slope between the soil stockpile and the pump station. 3934 MURPHY CANYON ROAD, SUITE B205, SAN DIEGO, CALIFORNIA 92123 (619) 292-8030 • (800) 447-2626 FAX (619) 292-0771 4901121-04 If you have any questions regarding our letter, please contact this office. We appreciate this opportunity to be of service. Respectfully submitted, LEIGHTON AND ASSOCIATES, INC. Lyne Perry Senior Staff Geologist LJP/lk Distribution: (1) Addressee (1) Regional Water Quality Control Board Attention: Mr. Jim Munch (1) City of Carlsbad Attention: Mr. Jay Hall -2- LEICHTON AND ASSOCIATES, INC Geotechnical and Environmental Engineering Consultants ADDITIONAL VERIFICATION SOIL SAMPLING AT THE AGUA HEDIONDA SEWAGE PUMP STATION, CARLSBAD, CALIFORNIA June 25, 1991 Project No. 4901121-04 Prepared For: CITY OF CARLSBAD 2075 Las Palmas Drive Carlsbad, California 92009 3934 MURPHY CANYON ROAD, SUITE B205, SAN DIEGO, CALIFORNIA 92123 (619) 292-8030 • (800) 447-2626 FAX (619) 292-0771 LEIGHTON AND ASSOCIATES, INC Geotechnical and Environmental Engineering Consultants June 25,1991 Project No. 4901121-04 To: City of Carlsbad 2075 Las Palmas Drive Carlsbad, California 92009 Attention: Mr. Jay Hall Subject: Additional Verification Soil Sampling at the Agua Hedionda Sewage Pump Station, Carlsbad, California Introduction Leighton and Associates, Inc. is pleased to submit this report which includes a discussion of the results of the additional verification soil sampling at the subject site. The objective of this additional soil sampling was to provide verification data as required by the San Diego Department of Health Services, Hazardous Materials Management Division (HMMD) in their letter dated May 9,1991, regarding the lateral extent of petroleum hydrocarbon contamination in the former fuel supply line trench. The scope of work for the subject investigation included collection of soil samples east, northeast, and south of the former fuel supply line trench, laboratory analyses of two soil samples, and preparation of this report. The following report includes a map showing the location of the soil samples, the results of the field investigation, a discussion of the laboratory results, and conclusions and recommendations. Accompanying Illustrations and Appendices Figure 1 - Site Location Map - Rear of Text Figure 2 - Location of Soil Samples - Rear of Text Figure 3 - Geologic Cross Section A-A' - Rear of Text Table 1 - Summary of Results of Laboratory Analyses - Rear of Text Appendix A - References Appendix B - Laboratory Analysis 3934 MURPHY CANYON ROAD, SUITE B205, SAN DIEGO, CALIFORNIA 92123 (619) 292-8030* (800) 447-2626 FAX (619) 292-0771 & 4901121-04 ^ Site Description and Background « The site is a sewage pump station that is part of a sewage pipeline system that boosts sewage J up to a topographically higher level so that it can be routed to a nearby treatment plant. The site is located near the south side of the Agua Hedionda lagoon, east of the railroad tracks and _ 2,500 feet northeast of the San Diego Gas and Electric (SDG&E) Encina Power Plant on Carlsbad J Boulevard (Figure 1). The site can be accessed via a dirt road which runs parallel with the railroad tracks and immediately east of the tracks. The dirt road can be accessed through the SDG&E plant. 4 In addition to being powered by electricity, the pump housed at the site has an emergency generator which is fueled by an underground diesel fuel storage tank. The emergency generator m is used to operate the pump station facility during interruptions in San Diego Gas and Electric 4 (SDG&E) electrical power service. According to City of Carlsbad representatives, the fuel tank was installed in 1977, and is 1,000 gallons in capacity and made of reinforced fiberglass. <i The City of Carlsbad had indicated to Leighton and Associates that a release had occurred from a pipe fitting in the fuel supply line from the tank to the generator. The release was discovered *" subsequent to removal of the tank and associated piping on July 25,1990. Subsequently, the «• city contracted Leighton and Associates to collect soil samples from the pipeline and tank excavation for analysis to evaluate which areas of soil had been contaminated by the release. ^ On July 25, 1990, Leighton and Associates collected two soil samples from the pipeline excavation (P-10-2' and P-21-2') at a depth of 2 feet below grade at the locations shown in — Figure 2. Each sample was analyzed by the laboratory for fuel hydrocarbons by Modified EPA Method 8015/DOHS. The results of these analyses are summarized in Table 1 and indicate that "" fuel hydrocarbons were not detected above the laboratory detection limit in soil sample P-10'-2. M However, fuel hydrocarbons were detected in soil sample P-21-2' at a concentration of 4,100mg/kg. „, As a result of the above data, the City of Carlsbad excavated the soil in the area of soil sample P-21-2' to a greater depth to remove hydrocarbon containing soil at a concentration above 100 * mg/kg (approximately 1 cubic yard). On August 9,1990, Leighton and Associates collected an additional soil sample (T-1-41) from the excavation in this area, and four soil samples (SP-1 through SP-4) from the stockpile produced by tank excavation. The soil samples were analyzed •* for fuel hydrocarbons and organic lead by EPA Method 6010. Soil samples T-1 -4' and SP-4 were also analyzed by EPA Method 8020 for benzene, toluene, ethylbenzene and total xylenes (BTEX). m The trench has been backfilled with clean soil and a building has been constructed over the 1 former diesel fuel line trench. The data indicates that fuel hydrocarbons and BTEX were not tf detected above the laboratory reported detection limit in soil sample T-1-4'. m m 4 4 i Hi 4901121-04 *• gi Field Investigation 2 On June 3, 1 991 , Leighton and Associates collected four soil samples south, east, and northeast of previously collected soil sample P-21 -2'. These soil samples were collected at depths of 2 and 3 feet below ground surface. Soil was first excavated to a depth of 1 foot utilizing a shovel. Soil ^ was then further excavated to depths of 2 to 3 feet utilizing a hand auger. The soil samples were j collected using a hand auger which was cleaned in a solution of trisodium phosphate (TSP) and *' water and rinsed with deionized water prior to the collection of each sample. After collection, each sample was placed in a laboratory supplied glass jar with a Teflon-lined cap and placed in 1 an ice-cooled container awaiting delivery to Analytical Technologies, Inc. (ATI) for analysis. The *" two samples located 2.5 feet east of the previous soil sample P-21 -2' were analyzed by the laboratory for fuel hydrocarbons by EPA Method 801 5/DOHS. Soil sample SS1 at 2 feet was ^ further analyzed for BTEX and organic lead by EPA Test Methods 8020 and 601 0, respectively. * The remaining soil samples were held for possible future analysis. m Visual or olfactory evidence of petroleum hydrocarbon contamination was not observed in the m soil samples. ** Verification soil samples could not be collected to the north or west of soil sample P-21 -2' due « to a recently constructed block building. *•» m Laboratory Results — The results of analytical analyses are summarized in Table 1 and presented in Appendix B. Chain-of-Custody forms and QA/QC data is also included in Appendix B. The data indicates that ** fuel hydrocarbons, BTEX, and organic lead were not detected above the laboratory reported «. detection limit in soil sample SS1 at 2 feet. In addition, fuel hydrocarbons were not detected above the laboratory reported detection limit in soil sample SS2 at 3 feet. m Conclusions and Recommendations« - Based on the results of this field investigation, the following conclusions and recommendations are presented. m Following the determination that 4,100 mg/kg (as diesel) of fuel hydrocarbons were previously m detected in soil sample P-21 -2', the excavation in the area of this sample was deepened to 4 feet. * Soil sample T-1 -4' was previously collected from the base of the trench and below the point where soil sample P-21 -2' was collected. Additional verification soil samples SS1 at 2 feet andm SS2 at 3 feet were collected on June 6, 1 991 , at 2.5 feet east of soil sample P-21 -2' in order to a define the lateral extent of hydrocarbon contamination. Fuel hydrocarbons were not detected in these samples. Therefore, it is our opinion that the petroleum hydrocarbon affected soil 1 (approximately 1 cubic yard) was removed from the trench excavation. - 3 - 4901121-04 •? •HI m Based upon the results of this investigation, we recommend no further action be performed at this time. The HMMD and RWQCB must agree with this recommendation before the City of Carlsbad can receive a site closure letter from these two regulatory agencies. Based on conversations with HMMD's case worker Mr. Mo Lahsaie at the site on May 24,1991, the stockpile soils (see Figure 2 for location) can be disposed of at a Class III Landfill (with HMMD and RWQCB approval letter) or can be utilized on site as fill material as long as the soils are not placed within 5 feet of the ground water table (i.e. their current location is greater than 15 feet above the water table) and are covered with clean fill soil to prevent volatization. If you have any questions regarding our report, please do not hesitate call us. We appreciate this opportunity to be of service. Respectfully submitted, LEIGHTON AND ASSOCIATES, INC. Lyne Perry Senior Staff Geologist Thomas E. Mills, RG 4439 Chief, Environmental Services LJP/TM/mw Distribution:(3) Addressee (1) County of San Diego Environmental Health Services Attention: Mr. Mo Lahsaie (1) Regional Water Quality Control Board Attention: Mr. Jim Munch - 4 - <tf m SITE LOCATION MAP Base Map: Aerial-Foto Map Book, 1986-87, page 7D Original by Aerial Graphics. AGUA HEDIONDA CITY OF CARLSBAD Project No 4901121-04 Date 6/25/91 1040 889 Figure No. 1 *—*- Former stockpile gravel and soil Excavation (5 yrds*) \ "_\ / \ I \ \ \ \ I Newly Constructed Building Gravel! Above ground tank | Soil / ssi e 2' iI' ISS2 9 3' I8'"2) Generator Former stockpile gravel and soil (9 yrds*) Stockpile ASP-6 LEGEND Soil sample location, SS1 « 2' designation, and depth in feet, collected on 6-3-91 SP-7 Relocated sol stockpile (9 yd*) and addttional soil from excavating activities in Jury and August 1990 (total 78 yd3) SP-8 JO Approximate Scale 4.0 feet 1-N-11.0' Soil sample location, designation and depth in feet, collected on 7-25-90 Soil sample location and designation, collected on 8-9-90 §Oj| sample location and designation, collected on 1-18-91 A' Cross section A-A' SOIL-SAMPLE LOCATIONS SEWAGE PUMP STATION Project No. 4901121-04 Scale 1fe20' Engr./Geol. JAH/LJP Drafted By JK Revised n 1042 839 Date e/oc/n-* I"*' °°y 4/19/91 6/25/91 RgureNo. 2 TABLE 1 SUMMARY OF RESULTS OF ANALYSIS OF SOILS SAMPLES Sample 1-N-11.0' 1-S-10.5 P-10-2' P-21-2' T-1-4' SP-1 SP-2 SP-3 SP-4 SP-5 SP-6 SP-7 SP-8 SS1 @ 2' SS2 @ 3' SS3 @ 2' SS4 @ 2' Date Sampled 7/25/90 7/25/90 7/25/90 7/25/90 8/9/90 8/9/90 8/9/90 8/9/90 8/9/90 1/18/90 1/18/90 1/18/91 1/18/91 6/3/91 6/3/91 6/3/91 6/3/91 Fuel Hydrocarbons(1 ) ND(5) ND ND 4,100 ND 300 ND 330 140 49 120 62 ND ND ND B(2) ND ND ND ND T(2) ND ND ND ND E(2) ND ND ND ND X(2) ND ND ND ND Organic Pb(3) ND ND ND ND ND ND ND Flash Point °F(4) >180 Explanation 0) (2) (3) (4) (5) * •m Fuel hydrocarbons by EPA Method 8015 (Modified)/DOHS Method BTEX - benzene, toluene, ethylbenzene, total xylenes by EPA Method 8020 Organic lead by EPA Method 6010/DOHS equivalent method Flash point in degrees Fahrenheit by EPA Method 1010 ND - Not detected at or above the laboratory detection limit Units in mg/kg Blank spaces indicated that compound was not analyzed for in the soil sample. 4901121-04 APPENDIX A - REFERENCES '* County of San Diego, Department of Health Services, Hazardous Material Management Division, m Site Assessment and Mitigation Manual, Section III, January 1991. ** Leighton and Associates, 1991, Revised Investigation of Subsurface and Stockpiled Soil Conditions at the Agua Hedionda Sewage Pump Station, Carlsbad, California, ** Project No. 4901121 -02, dated April 19. A-1 APPENDIX B /A\AnolyticalTechnologiesflnc.Corporate Offices: 555O Morehouse Drive San Diego, CA 92121 (619) 458-9141 ATI I.D.: 106012 June 11, 1991 * LEIGHXON & ASSOCIATES , 3934 MURPHY CYN RD., SUITE 205 B • SAN DIEGO, CA 92123 <•) Project Name: AQUA HEDIONDA — Project # : 4901121-003 Attention: LYNE PERRY*m & Analytical Technologies, Inc. has received the following sample (s): „, Date Received Quantity Matrix 4June 03, 1991 SOIL «. The sample(s) were analyzed with EPA methodology or equivalent methods as specified in the enclosed analytical schedule. The symbol for "less than" indicates a value below the reportable *"* detection limit. Please see the attached sheet for the sample cross reference table. *" The results of these analyses and the quality control data are enclosed. PR STEWART CT MANAGER-FUELS KENNETH WAHL LABORATORY MANAGER AAndy ticalTechnologies,! nc. SAMPLE CROSS REFERENCE Page 1 m Client : LEIOHTOM & ASSOCIATES Report Datet June 11, 1991 — Project # : 4901121-003 AXX I.O. : 106012 Project Name: AQUA HEDIONDA m _• AXI # Client Description Matrix Date Collected „ 1 SSI e 2* SOIL 03-JUN-91 2 SS2 8 3' SOIL 03-JUN-91 «* 3 SS3 0 2* SOIL 03-JUN-91 4 SS4 0 2' SOIL 03-JUN-91 •Bft • ^^^^^^^^^^••^^^^^^^^^^•^^^^^^^^^^B._,MlM^—•—••••-—••-••«•-—•«B«««^KW_»M«BBB^««• ^_»_»^_B_HM__ ^ ••••••!••••••••!••• ** TOTALS if SanplaK 4 ATI STANDARD DISPOSAL PRACTICE The sample(s) from this project will be disposed of in twenty-one (21) days from the date of this report. If an extended storage period is required, please contact our sample control department before the scheduled disposal date. ^ AnalyticalTechnologies,lnc. Client : LEIGHXON & ASSOCIATES Project # : 4901121-003 Project Name: AQUA HBDIONDA ANALYTICAL SCHEDULE Page 2 ATI I.D.: 106012 Analysis Technique/Description EPA 6010 (LEAD, ORGANIC) EPA 8020 (AROMATIC VOLATILE ORGANICS) MOD EPA 8015-CDOHS (FUEL HYDROCARBONS) INDUCTIVELY COUPLED ARGON PLASMA OC/ PHOTO IONIZATION DETECTOR GC/ FLAME IONIZATION DETECTOR AnalyticolTechnologies,lnc. Client : LEIOHTOH & ASSOCIATES Project # : 4901121-003 Project Name: AQUA HEDIONDA METALS RESULTS Page 3 ATI I.D.: 106012 Sample Client ID # Matrix Date Sampled Date Received 1 SSI 9 2' Parameter ORGANIC LEAD SOIL Units 1 MG/KG <0.3 03-JUN-91 03-JUN-91 /fj^ AnalyticalTechnologies,lnc. METALS - QUALITY CONTROL DUP/MS m Page 4 — Client: : LEIOHTON & ASSOCIATES m Project # : 4901121-003 ATI I.D. : 106012 Project Name: AQUA HEDIONDA 41 Parameters REF I.D. Units Sample Dup RPD Spiked Spike % Result Result Sample Cone Rec m ORGANIC LEAD 106012-01 MG/KO <0.3 <0.3 0 9.0 10.4 87 m % Recovery = (Spike Sample Result - Sample Result)*100/Spike Concentration m RPD (Relative % Difference) = (Sample Result - Duplicate Result)*100/Average Result AAnalyticalTechnologies,lnc. METALS - QUALITY CONTROL M BLANK SPIKE *• Page 5 „ Client : LEI6HTON & ASSOCIATES Project f : 4901121-003 ATI I.D. : 106012 Project Name: AQUA HEOIONDA 4 —Parameter* Blank Units Blank Spiked Spike % m Spike ID# Result Sample Cone. Rec *• ORGANIC LEAD 13661 M6/K6 <0.3 12.4 10.4 119 m % Recovery = (Spike Sample Result - Sample Result)*100/Spike Concentration RPD (Relative % Difference) = (Sample Result - Duplicate Result)*100/Average Result AnalyticalTechnologies,lnc. GAS CHROMATOGRAPHY RESULTS Page 6 Test : EPA 8020 (AROMATIC VOLATILE ORGANICS) Client : LEIGHTON & ASSOCIATES ATI I.D. : 106012 Project f : 4901121-003 Project Name: AQUA HEDIONDA Sample Client ID Matrix Date Date Date Oil. # Sampled Extracted Analyzed Factor 1 SSI e 2' SOIL 03-JUN-91 03-JUN-91 04-JUN-91 1.00 Parameter Units 1 BENZENE MG/KG <0.025 TOLUENE MG/KG <0.025 ETHYLBENZENE MG/KG <0.025 ZYLENES (TOTAL) MG/KG <0.050 SURROGATES TRIFLUOROTOLUENE % 112 X\AnalyticalTeehnologies,lnc. GAS CHROHATOGRAPHY - QUALITY CONTROL REAGENT BLANK m M 11 m I *t m Test Blank I.D. Client Project # Project Name Parameters BENZENE TOLUENE ETHYLBENZENE EPA 8020 (AROMATIC VOLATILE ORGANICS) 12460 LEIGHTON & ASSOCIATES 4901121-003 AQUA HEDIONDA ZYLENES (TOTAL) Units MG/KG MG/KG MG/KG MG/KG ATI I.D. : Date Extracted: Date Analyzed : Oil . Factor : Page 7 106012 03-JUN-91 03-JUN-91 1.00 Results <0 <0 <0 <0 .025 .025 .025 .050 SURROGATES TRIFLUOROTOLUENE 110 <** ^J^ Anolyt calTechnologies,!nc. m GAS CHROMATOGRAPHY - QUALITY CONTROLM MSMSD *• Page 8 — Test EPA 8020 (AROMATIC VOLATILE ORGANICS) ATI I.D. : 106012 MSMSD # 15781 Date Extracted: 03-JUN-91 Client ^ Project t Project Name Parametersm *• BENZENE TOLUENE ** % Recovery * — RPD (Relative LEIGHTON & ASSOCIATES 4901121-003 AQUA HEDIONDA Units MG/KG MG/KG Date Analysed : 03-JUN-91 Sample Matrix : SOIL REF I.D. t 105355-14 Sample Result <0.025 <0.025 Cone Spiked Spike Sample 0.500 0.54 0.500 0.54 Rec 108 108 Dup Spike 0.55 0.55 Dup % Rec 110 110 (Spike Sample Result - Sample Result )*100/ Spike Concentration % Difference) = (Spiked Sample Result - Duplicate Spike Result) *100/ Average RPD 2 2 Result AnalyticalTechnologies,lnc Test : Blank Spike #: Client : Project # : Project Name : OAS CHROMATOGRAPHY - QUALITY CONTROL BLANK SPIKE EPA 8020 (AROMATIC VOLATILE ORGAN! CS) 13439 LEIOHTON & ASSOCIATES 4901121-003 AQUA HEDIONDA ATI I.D. : Date Extracted: Date Analyzed : Sample Matrix : Page 9 106012 03-JUN-91 03-JUN-91 SOIL Parameters m BENZENE TOLUENE Units MG/KG MG/KG Blank Result <0.025 <0.025 Spiked Sample 0.58 0.57 Spike Cone. 0.500 0.500 Rec 116 114 % Recovery = (Spike Sample Result - Sample Result)*100/Spike Concentration RPD (Relative % Difference) = (Spiked Sample - Blank Result)*100/Average Result AnalyticalTechnologies,lnc. GAS CHROMATOGRAPHY RESULTS ** Page 10 Test t MOD EPA 8015-CDOHS (FUEL HYDROCARBONS) •* Client : LEIGHTON & ASSOCIATES ATI I.D. t 106012 — Project # : 4901121-003 Project Name: AQUA HEDIONDA * Sample Client ID Matrix Date Date Date Dil. jtf # Sampled Extracted Analyzed Factor m 1 SSI 6 2* SOIL 03-JUN-91 03-JUN-91 06-JUN-91 1.00 2 SS2 8 3' SOIL 03-JUN-91 03-JUN-91 06-JUN-91 1.00 Parameter Units 1 2 . FUEL HYDROCARBONS MG/KG <5.0 <5.0 HYDROCARBON RANGE HYDROCARBONS QUANTITATED USING AnalyticalTechnologies,lnc gg Test Blank I.D. Client ** Project # 4f Project Name GAS CHROMATOGRAPHY - QUALITY CONTROL REAGENT BLANK MOD EPA 8015-CDOHS (FUEL HYDROCARBONS) 12515 LEIGHTON & ASSOCIATES 4901121-003 AQUA HEDIONDA Page 11 ATI I.D. : 106012 Date Extracted: 03-JUN-91 Date Analyzed : 06-JUN-91 Oil. Factor : 1.00 Parameters FUEL HYDROCARBONS HYDROCARBON RANGE HYDROCARBONS QUANTITATED USING Units NG/KG Results <5.0 <m m AnalyticalTechnologies,lnc. GAS CHRONATOORAPHY - QUALITY CONTROL Test NSNSD # Client NSMSD : MOD EPA 8015-CDOHS (FUEL HYDROCARBONS) : 15901 : LEIGHTON & ASSOCIATES tff Project # : 4901121-003 Project Name: AQUA HBDIONDA Page 12 ATI I.D. : 106012 Date Extracted: 03-JUN-91 Date Analyzed : 06-JUN-91 Sample Matrix : SOIL REF I.D. : 106012-01 Parameters Units Sample Result Cone Spike Spiked Sample % Rec Dup Spike Dup RPD % Rec *• FUEL HYDROCARBONS MG/KG <5.0 100 88 88 88 88 % Recovery = (Spike Sample Result - Sample Result)*100/Spike Concentration RPD (Relative % Difference) = (Spiked Sample Result - Duplicate Spike Result)*100/Average Result $± AnalyticalTechnologies,lnc. GAS CHROMATOGRAPHY - QUALITY CONTROL BLANK SPIKE Test : MOD EPA 8015-CDOHS (FUEL HYDROCARBONS) Blank Spike #: 13525 Client : LEIGHTON & ASSOCIATES Project # J 4901121-003 Project Name : AQUA HEDIONDA Page 13 ATI I.D. : 106012 Date Extracted: 03-JUN-91 Date Analyzed : 06-JUN-91 Sample Matrix : SOIL Paraaeters FUEL HYDROCARBONS Units MG/KG Blank Result <S.O Spiked Sample 91 Spike Cone. 100 % Rec 91 % Recovery = (Spike Sample Result - Sample Result)*100/Spike Concentration RPD (Relative % Difference) - (Spiked Sample - Blank Result)*100/Average Result tilJtitJiitjtii 5550 MOREHOUSE DRIVE ^ AndyticalTechnologies, Inc. t. j fc| ft __ - - Cfiaif) O/DATE.E_L OF_l_ Recommended Quantity and Preservative (Provide triple volume on QC Sample^. DISTRIBUTION: White, Canary • ANALYTICAL TECHNOLOGIES, INC. • Pink- ORIGINAfQR