HomeMy WebLinkAboutCT 12-01; Miles Pacific Subdivision; Tentative Map (CT) (3).. Page 1 of 7
(;a/science
C_nvironmental
jj i. aboratories, Inc.
June 16, 2011
Bryan Voss
GeoSoils, Inc.
5741 Palmer Way
Carlsbad, CA 92010-7248
Subject: Calscience Work Order No.: 11-06-0692
Client Reference: Miles-Pacific, LP
Dear Client:
Enclosed is an analytical report for the above-referenced project. The samples included
in this report were received 6/9/2011 and analyzed in accordance with the attached
chain-of-custody.
Calscience Environmental Laboratories certifies that the test results provided in this
report meet all NELAC requirements for parameters for which accreditation is required
or available. Any exceptions to NELAC requirements are noted in the case narrative.
The original report of subcontracted analysis, if any, is provided herein, and follows the
standard Calscience data package. The results in this analytical report are limited to the
samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report, please do not hesitate to contact the
undersigned.
Sincerely,
Calscience Environmental
Laboratories. Inc.
Richard Villafania
Project Manager
.Ia 1 NELAP 10: 03220CA • OoO-ELAP 10 L 10-41 • CSOLAC 10 10109 • SCAQMO 10: 93LA0830
~ 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501
----------------------------------------------------------------------------------,
---l._i!lscience
#i = nvironmental
I . -aboratones, Inc.
GeoSoils, Inc.
5741 Palmer Way
Carlsbad, CA 92010-7248
Project: Miles-Pacific, LP
Client Sample Number
S-3@3'
Parameter
Aldrin
Alpha-BHC
Beta-BHC
Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Delta-BHC
Dieldrin
Endosulfan I
Surrogates:
Decachlorobiphenyl
Method Blank
Parameter
Aldrin
Alpha-BHC
Beta-BHC
Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Delta-BHC
Dieldrin
Endosulfan I
Surrogates:
Decachlorobiphenyl
Result
ND
ND
ND
ND
ND
55
21
ND
ND
ND
REC(%)
70
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RECI%\
70
RL
5.0
5.0
5.0
50
5.0
10
5.0
5.0
5.0
5.0
Control
Limits
50-135
RL
5.0
5.0
5.0
50
5.0
5.0
5.0
5.0
5.0
5.0
QQn1[Ql
Limits
50-135
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
Units:
Lab Sample Date!Time
Number Collected Matrix Instrument
11.06.0692-1-A 06109/11 Solid GC51
11:00
DF QYID Paramet!ilr
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Endrin Ketone
2 Gamma-BHC
1 Heptachlor
1 Heptachlor Epoxide
Methoxychlor
Toxaphene
QYID Surrogajes:
2,4 ,5,6-T etrachloro-m-Xylene
099-12-537-1,047 N/A Solid GC51
DF Qual Parameter
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Endrin Ketone
Gamma-BHC
Heptachlor
Heptachlor Epoxide
1 Methoxychlor
1 Toxaphene
QYID S!,!rrogates:
2,4,5,6-Tetrachloro-m-Xylene
.I a I RL -RepOrting Limit ' DF -Dilution Factor ' Qual -Qualifiers
Page 2 of 7
06/09/11
11-06-0692
EPA 3545
EPA 8081A
ug/kg
Page 1 of 1
Date Date!Time
Prepared Analyzed QC Batch ID
06/10/11 06/14111 110610L16
20:43
Result RL DF QYID
ND 5.0 1
ND 5.0 1
ND 5.0
ND 5.0
ND 5.0
ND 5.0 1
ND 5.0 1
ND 5.0 1
ND 5.0 1
160 100 1
REC (%) Control Q.!.!2!
Limjjs
79 50-135
06/10/11 06/14111 110610L16
15:40
Result RL DF QYID
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0 1
ND 100 1
~ Control Q.!.!.ill
Limjjs
95 50-135
~ 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501
1.= a/science
C_nvironmental Quality Control -Spike/Spike Duplicate
L aboratories, Inc.
GeoSoils, Inc.
57 41 Palmer Way
Carlsbad, CA 92010-7248
Project Miles-Pacific, LP
Quality Control Sample ID
111..()6..()708-9
Parameter
Aldrin
Alpha-BHC
Beta-BHC
4,4'-DDD
4,4'-DDE
4,4'-DDT
Delta-BHC
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Gamma-BHC
Heptachlor
Heptachlor Epoxide
Methoxychlor
Matrix
Solid
MS%REC
77
80
84
82
82
86
82
78
76
80
75
85
65
83
80
70
79
RPD-Relative Percent Difference , CL -Control Limit
Date Received:
Work Order No:
Preparation:
Method:
Date Instrument Prepared
GC51 06/10/11
MSD%REC %REC CL RPD
70 50-135 10
73 50-135 9
78 50-135 7
81 50-135 1
81 50-135 2
79 50-135 9
75 50-135 9
76 50-135 3
74 50-135 2
79 50-135
72 50-135 5
80 50-135 6
64 50-135 2
77 50-135 7
75 50-135 6
70 50-135 0
71 50-135 11
Page 3 of 7
Date
Analyzed
06/14/11
RPDCL
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
06/09/11
11-06-0692
EPA 3545
EPA 8081A
MS/MSD Batch
Number
110610816 I
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501
--.. a/science
t _nvironmental Quality Control -LCS/LCS Duplicate
L aboratories, Inc.
GeoSoils, Inc.
5741 Palmer Way
Carlsbad, CA 92010-7248
Project: Miles-Pacific, LP
Quality Control Sample ID
099-12-537-1,047
Parameter
Aldrin
Alpha-BHC
Beta-BHC
4,4'-DDD
4,4'-DDE
4,4'-DDT
Delta-BHC
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Gamma-BHC
Heptachlor
Heptachlor Epoxide
Methoxychlor
Total number of LCS compounds : 17
Total number of ME compounds : 0
Total number of ME compounds allowed :
LCS ME CL validation result : Pass
Matrix
Solid
LCS %REC
87
93
97
94
95
99
93
92
91
94
89
101
83
97
94
79
94
RPD-Relative Percent Difference , CL-Control Limit
Date Received:
Work Order No:
Preparation:
Method:
Date Date
Instrument Prepared Analyzed
GC51 06/10/11 06114111
LCSD %REC %REC CL ME CL RPD
91 50-135 36-149 5
94 50-135 36-149 2
96 50-135 36-149
90 50-135 36-149 4
93 50-135 36-149 3
98 50-135 36-149
93 50-135 36-149 0
90 50-135 36-149 2
90 50-135 36-149
92 50-135 36-149 2
88 50-135 36-149
101 50-135 36-149
82 50-135 36-149 1
97 50-135 36-149 0
95 50-135 36-149
77 50-135 36-149 2
94 50-135 36-149 0
Page 4 of 7
N/A
11-06-0692
EPA 3545
EPA 8081A
LCS/LCSD Batch
Number
110610L16
RPDCL Qualifiers
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501
Page 5 of 7
..,;;;;;;;,. --. 1. a/sctence
t_nvironmental
6 Glossary of Terms and Qualifiers
II. aboratories, Inc.
Work Order Number: 11-06-0692
Qualifier
*
<
>
1
2
3
4
5
6
7
B
BU
E
ET
J
ME
ND
Q
X
z
Definition
See applicable analysis comment.
Less than the indicated value.
Greater than the indicated value.
Surrogate compound recovery was out of control due to a required sample dilution,
therefore, the sample data was reported without further clarification.
Surrogate compound recovery was out of control due to matrix interference. The
associated method blank surrogate spike compound was in control and, therefore, the
sample data was reported without further clarification.
Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out
of control due to matrix interference. The associated LCS and/or LCSD was in control
and, therefore, the sample data was reported without further clarification.
The MS/MSD RPD was out of control due to matrix interference. The LCS/LCSD RPD
was in control and, therefore, the sample data was reported without further clarification.
The PDS/PDSD or PES/PESD associated with this batch of samples was out of control
due to a matrix interference effect. The associated batch LCS/LCSD was in control and,
hence, the associated sample data was reported without further clarification.
Surrogate recovery below the acceptance limit.
Surrogate recovery above the acceptance limit.
Analyte was present in the associated method blank.
Sample analyzed after holding time expired.
Concentration exceeds the calibration range.
Sample was extracted past end of recommended max. holding time.
Analyte was detected at a concentration below the reporting limit and above the
laboratory method detection limit. Reported value is estimated.
LCS Recovery Percentage is within LCS ME Control Limit range.
Parameter not detected at the indicated reporting limit.
Spike recovery and RPD control limits do not apply resulting from the parameter
concentration in the sample exceeding the spike concentration by a factor of four or
greater.
% Recovery and/or RPD out-of-range.
Analyte presence was not confirmed by second column or GC/MS analysis.
Solid-Unless otherwise indicated, solid sample data is reported on a wet weight basis, not
corrected for % moisture. All QC results are reported on a wet weight basis.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501
'-£ L
Calscience Environmerftal Laboratories, Inc.
M SoCallaboratory 0 NorCal Service Center r 7440 lincoln Way 5063 Commercial Circle, Suite H
Garden Grove. CA 92841-1427 Concord, CA 94520-8577
(714) 895-5494 (925) 689-9022
SPECIAL REQUIREMENTS (ADDITIONAL COSTS MAY APPLY)
0 RWQCB REPORTING FORMS 0 COEL T EOF 0
SPECIAL INSTRUCTIONS:
-:t.C ~~-5-3e"B 1 1~ Clbe Lc~=>o~)l.__,
~ lo't49~ j ~ ScvAt>le a 5-3 e. 4. ~' pJ~.
SAMPLE 10 FIELD POINT NAME
(FOR COEL T EDF)
DISTRIBUTION: White with fmal report, Green and Yellow to Client.
Please note that pages 1 and 2 of 2 of our TICs are printed on the reverse side of the green and Yelow copies respectively.
CHAfN OF CUSTODY RECORD
Date ~ 2611
Page
COELT LOG CODE
DODD
05/01/07 Revision
Page 7 of 7
WORK ORDER#: 11-06· [g ~ ~ ~
SAMPLE RECEIPT FORM Cooler _j_ of _j_
DATE: 06 I 111 CLIENT: ----=G~e J.L,.U ~5IL..IO 1-t:.£-_)~--
TEMPERATURE: Thermometer 10: SC1 (Criteria: 0.0°C-6.0°C, not frozen)/ ·
Temperature IJ-._j_ °C + 0.5 °C (CF) = 2--. .j__ °C fi Blank · 0 Sample
0 Sample(s) outside temperature criteria (PM/APM contacted by: ).
0 Sample{s) outside temperature criteria but received on ice/chilled on same day of sampling.
0 Received at ambient temperature, placed on ice for transport by Courier.
Ambient Temperature: 0 Air 0 Filter Initial: -..1--+l-f-
CUSTODY SEALS INTACT:
0 Cooler 0 ____ _
o Sample o ____ _
o No (Not Intact)
o No (Not Intact)
Ill ~ot Present
(S(Not Present
0 N/A
SAMPLE CONDITION: Yes
Chain-Of-Custody (COC) document(s) received with samples ................... fi ·
COC document(s) received complete ................................................... Ei"
0 Collection date/time, matrix, and/or# of containers Jogged in based on sample labels.
0 No analysis requested. 0 Not relinquished. 0 No date/time relinquished. /
Sampler's name indicated on COC ...................................................... 'eJ /
Sample container label(s) consistent with COC ...................................... &1
Sample container(s) intact and good condition ....................................... ~
Proper containers and sufficient volume for analyses requested ................ ~
Analyses received within holding time .................................................. ~
pH I Res. Chlorine I Diss. Sulfide I Diss. Oxygen received within 24 hours ... 0
Proper preservation noted on COC or sample container...... . . . . . . . . . . . . . . . . . . . . o
0 Unpreserved vials received for Volatiles analysis
Volatile analysis container(s) free of headspace ..................................... 0
Tedlar bag(s) free of condensation ...................................................... o CONTAI~R TYPE:
No
0
0
0
0
0
0
0
0
0
0
0
Initial: _&11_
lnltiai:L
N/A
0
0
0
0
0
0
Solid: ~ozCGJ 08ozCGJ 016ozCGJ OSieeve ( ) OEnCores® OTerraCores® 0 __ _
Water: OVOA OVOAh OVOAna2 0125AGB 0125AGBh 0125AGBp 01AGB 01AGBna2 01AGBs
0500AGB 0500AGJ 0500AGJs 0250AGB 0250CGB 0250CGBs 01PB 0500PB 0500PBna
0250PB 0250PBn 0125PB 0125PBznna 0100PJ 0100PJnaz 0 0 0 __ _
Air: OTedlar® OSumma® Other: 0 Trip Blank Lot#: Labeled/Checked by: /W
Container: C: Clear A: Amber P: Plastic G: Glass J: Jar B: Bottle Z: Ziploc/Resealable Bag E: Envelope Reviewed by:?~l:;rrv:;;:::_j~
Preservative: h: HCL n: HN03 na2:NazS203 na: NaOH p: H3P04 s: Hz504 znna: ZnAcz+NaOH f: Field-filtered Scanned by: TJ;/
SOP T100_090 (03124/11)