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HomeMy WebLinkAboutCT 12-01; Miles Pacific Subdivision; Tentative Map (CT) (3).. Page 1 of 7 (;a/science C_nvironmental jj i. aboratories, Inc. June 16, 2011 Bryan Voss GeoSoils, Inc. 5741 Palmer Way Carlsbad, CA 92010-7248 Subject: Calscience Work Order No.: 11-06-0692 Client Reference: Miles-Pacific, LP Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 6/9/2011 and analyzed in accordance with the attached chain-of-custody. Calscience Environmental Laboratories certifies that the test results provided in this report meet all NELAC requirements for parameters for which accreditation is required or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analysis, if any, is provided herein, and follows the standard Calscience data package. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Sincerely, Calscience Environmental Laboratories. Inc. Richard Villafania Project Manager .Ia 1 NELAP 10: 03220CA • OoO-ELAP 10 L 10-41 • CSOLAC 10 10109 • SCAQMO 10: 93LA0830 ~ 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501 ----------------------------------------------------------------------------------, ---l._i!lscience #i = nvironmental I . -aboratones, Inc. GeoSoils, Inc. 5741 Palmer Way Carlsbad, CA 92010-7248 Project: Miles-Pacific, LP Client Sample Number S-3@3' Parameter Aldrin Alpha-BHC Beta-BHC Chlordane 4,4'-DDD 4,4'-DDE 4,4'-DDT Delta-BHC Dieldrin Endosulfan I Surrogates: Decachlorobiphenyl Method Blank Parameter Aldrin Alpha-BHC Beta-BHC Chlordane 4,4'-DDD 4,4'-DDE 4,4'-DDT Delta-BHC Dieldrin Endosulfan I Surrogates: Decachlorobiphenyl Result ND ND ND ND ND 55 21 ND ND ND REC(%) 70 Result ND ND ND ND ND ND ND ND ND ND RECI%\ 70 RL 5.0 5.0 5.0 50 5.0 10 5.0 5.0 5.0 5.0 Control Limits 50-135 RL 5.0 5.0 5.0 50 5.0 5.0 5.0 5.0 5.0 5.0 QQn1[Ql Limits 50-135 Analytical Report Date Received: Work Order No: Preparation: Method: Units: Lab Sample Date!Time Number Collected Matrix Instrument 11.06.0692-1-A 06109/11 Solid GC51 11:00 DF QYID Paramet!ilr Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone 2 Gamma-BHC 1 Heptachlor 1 Heptachlor Epoxide Methoxychlor Toxaphene QYID Surrogajes: 2,4 ,5,6-T etrachloro-m-Xylene 099-12-537-1,047 N/A Solid GC51 DF Qual Parameter Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone Gamma-BHC Heptachlor Heptachlor Epoxide 1 Methoxychlor 1 Toxaphene QYID S!,!rrogates: 2,4,5,6-Tetrachloro-m-Xylene .I a I RL -RepOrting Limit ' DF -Dilution Factor ' Qual -Qualifiers Page 2 of 7 06/09/11 11-06-0692 EPA 3545 EPA 8081A ug/kg Page 1 of 1 Date Date!Time Prepared Analyzed QC Batch ID 06/10/11 06/14111 110610L16 20:43 Result RL DF QYID ND 5.0 1 ND 5.0 1 ND 5.0 ND 5.0 ND 5.0 ND 5.0 1 ND 5.0 1 ND 5.0 1 ND 5.0 1 160 100 1 REC (%) Control Q.!.!2! Limjjs 79 50-135 06/10/11 06/14111 110610L16 15:40 Result RL DF QYID ND 5.0 ND 5.0 ND 5.0 ND 5.0 ND 5.0 ND 5.0 ND 5.0 ND 5.0 ND 5.0 1 ND 100 1 ~ Control Q.!.!.ill Limjjs 95 50-135 ~ 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501 1.= a/science C_nvironmental Quality Control -Spike/Spike Duplicate L aboratories, Inc. GeoSoils, Inc. 57 41 Palmer Way Carlsbad, CA 92010-7248 Project Miles-Pacific, LP Quality Control Sample ID 111..()6..()708-9 Parameter Aldrin Alpha-BHC Beta-BHC 4,4'-DDD 4,4'-DDE 4,4'-DDT Delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Gamma-BHC Heptachlor Heptachlor Epoxide Methoxychlor Matrix Solid MS%REC 77 80 84 82 82 86 82 78 76 80 75 85 65 83 80 70 79 RPD-Relative Percent Difference , CL -Control Limit Date Received: Work Order No: Preparation: Method: Date Instrument Prepared GC51 06/10/11 MSD%REC %REC CL RPD 70 50-135 10 73 50-135 9 78 50-135 7 81 50-135 1 81 50-135 2 79 50-135 9 75 50-135 9 76 50-135 3 74 50-135 2 79 50-135 72 50-135 5 80 50-135 6 64 50-135 2 77 50-135 7 75 50-135 6 70 50-135 0 71 50-135 11 Page 3 of 7 Date Analyzed 06/14/11 RPDCL 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 06/09/11 11-06-0692 EPA 3545 EPA 8081A MS/MSD Batch Number 110610816 I Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501 --.. a/science t _nvironmental Quality Control -LCS/LCS Duplicate L aboratories, Inc. GeoSoils, Inc. 5741 Palmer Way Carlsbad, CA 92010-7248 Project: Miles-Pacific, LP Quality Control Sample ID 099-12-537-1,047 Parameter Aldrin Alpha-BHC Beta-BHC 4,4'-DDD 4,4'-DDE 4,4'-DDT Delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Gamma-BHC Heptachlor Heptachlor Epoxide Methoxychlor Total number of LCS compounds : 17 Total number of ME compounds : 0 Total number of ME compounds allowed : LCS ME CL validation result : Pass Matrix Solid LCS %REC 87 93 97 94 95 99 93 92 91 94 89 101 83 97 94 79 94 RPD-Relative Percent Difference , CL-Control Limit Date Received: Work Order No: Preparation: Method: Date Date Instrument Prepared Analyzed GC51 06/10/11 06114111 LCSD %REC %REC CL ME CL RPD 91 50-135 36-149 5 94 50-135 36-149 2 96 50-135 36-149 90 50-135 36-149 4 93 50-135 36-149 3 98 50-135 36-149 93 50-135 36-149 0 90 50-135 36-149 2 90 50-135 36-149 92 50-135 36-149 2 88 50-135 36-149 101 50-135 36-149 82 50-135 36-149 1 97 50-135 36-149 0 95 50-135 36-149 77 50-135 36-149 2 94 50-135 36-149 0 Page 4 of 7 N/A 11-06-0692 EPA 3545 EPA 8081A LCS/LCSD Batch Number 110610L16 RPDCL Qualifiers 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501 Page 5 of 7 ..,;;;;;;;,. --. 1. a/sctence t_nvironmental 6 Glossary of Terms and Qualifiers II. aboratories, Inc. Work Order Number: 11-06-0692 Qualifier * < > 1 2 3 4 5 6 7 B BU E ET J ME ND Q X z Definition See applicable analysis comment. Less than the indicated value. Greater than the indicated value. Surrogate compound recovery was out of control due to a required sample dilution, therefore, the sample data was reported without further clarification. Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound was in control and, therefore, the sample data was reported without further clarification. Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to matrix interference. The associated LCS and/or LCSD was in control and, therefore, the sample data was reported without further clarification. The MS/MSD RPD was out of control due to matrix interference. The LCS/LCSD RPD was in control and, therefore, the sample data was reported without further clarification. The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to a matrix interference effect. The associated batch LCS/LCSD was in control and, hence, the associated sample data was reported without further clarification. Surrogate recovery below the acceptance limit. Surrogate recovery above the acceptance limit. Analyte was present in the associated method blank. Sample analyzed after holding time expired. Concentration exceeds the calibration range. Sample was extracted past end of recommended max. holding time. Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is estimated. LCS Recovery Percentage is within LCS ME Control Limit range. Parameter not detected at the indicated reporting limit. Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spike concentration by a factor of four or greater. % Recovery and/or RPD out-of-range. Analyte presence was not confirmed by second column or GC/MS analysis. Solid-Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are reported on a wet weight basis. 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501 '-£ L Calscience Environmerftal Laboratories, Inc. M SoCallaboratory 0 NorCal Service Center r 7440 lincoln Way 5063 Commercial Circle, Suite H Garden Grove. CA 92841-1427 Concord, CA 94520-8577 (714) 895-5494 (925) 689-9022 SPECIAL REQUIREMENTS (ADDITIONAL COSTS MAY APPLY) 0 RWQCB REPORTING FORMS 0 COEL T EOF 0 SPECIAL INSTRUCTIONS: -:t.C ~~-5-3e"B 1 1~ Clbe Lc~=>o~)l.__, ~ lo't49~ j ~ ScvAt>le a 5-3 e. 4. ~' pJ~. SAMPLE 10 FIELD POINT NAME (FOR COEL T EDF) DISTRIBUTION: White with fmal report, Green and Yellow to Client. Please note that pages 1 and 2 of 2 of our TICs are printed on the reverse side of the green and Yelow copies respectively. CHAfN OF CUSTODY RECORD Date ~ 2611 Page COELT LOG CODE DODD 05/01/07 Revision Page 7 of 7 WORK ORDER#: 11-06· [g ~ ~ ~ SAMPLE RECEIPT FORM Cooler _j_ of _j_ DATE: 06 I 111 CLIENT: ----=G~e J.L,.U ~5IL..IO 1-t:.£-_)~-- TEMPERATURE: Thermometer 10: SC1 (Criteria: 0.0°C-6.0°C, not frozen)/ · Temperature IJ-._j_ °C + 0.5 °C (CF) = 2--. .j__ °C fi Blank · 0 Sample 0 Sample(s) outside temperature criteria (PM/APM contacted by: ). 0 Sample{s) outside temperature criteria but received on ice/chilled on same day of sampling. 0 Received at ambient temperature, placed on ice for transport by Courier. Ambient Temperature: 0 Air 0 Filter Initial: -..1--+l-f- CUSTODY SEALS INTACT: 0 Cooler 0 ____ _ o Sample o ____ _ o No (Not Intact) o No (Not Intact) Ill ~ot Present (S(Not Present 0 N/A SAMPLE CONDITION: Yes Chain-Of-Custody (COC) document(s) received with samples ................... fi · COC document(s) received complete ................................................... Ei" 0 Collection date/time, matrix, and/or# of containers Jogged in based on sample labels. 0 No analysis requested. 0 Not relinquished. 0 No date/time relinquished. / Sampler's name indicated on COC ...................................................... 'eJ / Sample container label(s) consistent with COC ...................................... &1 Sample container(s) intact and good condition ....................................... ~ Proper containers and sufficient volume for analyses requested ................ ~ Analyses received within holding time .................................................. ~ pH I Res. Chlorine I Diss. Sulfide I Diss. Oxygen received within 24 hours ... 0 Proper preservation noted on COC or sample container...... . . . . . . . . . . . . . . . . . . . . o 0 Unpreserved vials received for Volatiles analysis Volatile analysis container(s) free of headspace ..................................... 0 Tedlar bag(s) free of condensation ...................................................... o CONTAI~R TYPE: No 0 0 0 0 0 0 0 0 0 0 0 Initial: _&11_ lnltiai:L N/A 0 0 0 0 0 0 Solid: ~ozCGJ 08ozCGJ 016ozCGJ OSieeve ( ) OEnCores® OTerraCores® 0 __ _ Water: OVOA OVOAh OVOAna2 0125AGB 0125AGBh 0125AGBp 01AGB 01AGBna2 01AGBs 0500AGB 0500AGJ 0500AGJs 0250AGB 0250CGB 0250CGBs 01PB 0500PB 0500PBna 0250PB 0250PBn 0125PB 0125PBznna 0100PJ 0100PJnaz 0 0 0 __ _ Air: OTedlar® OSumma® Other: 0 Trip Blank Lot#: Labeled/Checked by: /W Container: C: Clear A: Amber P: Plastic G: Glass J: Jar B: Bottle Z: Ziploc/Resealable Bag E: Envelope Reviewed by:?~l:;rrv:;;:::_j~­ Preservative: h: HCL n: HN03 na2:NazS203 na: NaOH p: H3P04 s: Hz504 znna: ZnAcz+NaOH f: Field-filtered Scanned by: TJ;/ SOP T100_090 (03124/11)