HomeMy WebLinkAboutCT 15-08; CARLSBAD RANCH PA 5 PHASE 3; LAB REPORTS; 2016-05-03US (ECOLOGY
'e Crxlel
EPA 10. ACOO8564S6
Addre: IP INrn' GPADT, IM
S420 QT4AW PACIFIC DRIVE
FA1RO)<. CA 9202
Ifli1t. O1SU2SJJK
Dzta-, 05103IM16
Tune In: S:48:54
rw= Out: 16:2326
RuWrr(p #: 42244
TrccthrfTrI#: 140g Ina
Quamy Of -r Sze CC!D CO~-
rrit /0702$3OC-319) 11 11 DM55 , 4, 5, 6, 7, 8, 9,
Ad1fl$OrnI Information;
/ erov g'ee t'it t?ie above fisted services and quantities are accurate,
ereseve: c
(Printed) (Signature) (The)
US CIO4y
senthe v /
(Printed) (S1gnciro)
j ZI ble caftadmatm Ewh LISENS tLte tfr$ai 1beet1l e
Pago 1 of 1
Please ptint or type, (Foft clesiqtd for use on elite (12-pitch) ttpewritet) Form Aptovéd. OMB No. 2050-0039
UNIFORM HAZARDOUS 1. Gerieiator ID Nun/be
. • tJ r5./4
2. Page 1 of 3, Emergeitcy Response Reese 14. Manifest Tracking Number
. -. ,.•
WASTE MANIFEST ' - - JJ K
5. Generators Name and Mailing Address , 5 qec.3 Generator's SiteAddress (if diiferenttharr mailing address)
!O. tt.2.A i.: br) (M)('p,:tK. UFtt/i
A ir t rr>o .
Generators Phone:
. 'ansporter 1 Company Name U.S. EPA ID Number
flh1 ?)AL RVL I
7. Transporter 2 Company Name . . U.S. EPA ID Nuhiber
S. Designated Facility Name and Site Address i, j. U. - U.S. EPA ID Number
-
Fact/tv's Phone: . '
qa 9b. U.S. DOT Description (including Proper Shipping Name, Hazard Class, ID Number, 10. Containers ii. Total 12. Unit as e Codes 13. Waste
. No. Type HM and Packing Group (if any)). . ., Quantity W001..
- 1_ Jf kfttU-fativ- r fl3 Wi tjfl ()'i :44 /
2. LU
.._
4. Special Hpndlh,g Irmtncttvntiand Additional information t'rjyn
GENERATOR'S/OFFEROR'S CERTIFtCA11ON I hereby declare that the contents of this consignment are billy and accurately described above by the proper shipping name, and are classified, packaged,
marked and labeled/placarded, and are in all respects in proper condition for transport according to applicable international and national governmental regulations. If export shipment and I am the Primary
Exporter, I certify that the contents of this consignment conform to the terms of the attached EPA Acknowledgment of Consent.
I certify that the waste minimization statement identified in 40 CFR 262.27(a) (if lam a large quantify generator) or (b) (if I am small quantity generator) is true.
j J
GeneratorsiOfferors PrintediTyped tame Signature Month Day3 Year
J fti-prrratioj/ai Snlpmerrts................. Import to U.S. Export from U.S. Port of entry/exit:
Transpdrters.lgnatu/e (for exports only'): . . Date leaving U.S.:
Transporter Acknowledgment of Receipt of Materials
Trantiports1 Printedflyped Name Signature,L , Month., Day,,, Year
CL I I (I, Z Transporter 2 Printed/Typed Name Signature - . Month Day Year
Ce —
Discrepahcy . . . . . . .
18a, Discrepancy Indication Space [II] Quantity [III Type 0 Residue E Partial Rejection [III] Full Rejection
Manifest Reference Number:
18b. Alternate Facifity. for Gnaralor) U.S. EPA ID Number
—J
I Fno8it'e Phone:
ir.sture otAiternate Ftrcttilycrr Ganator) . Month Day Year
II
LLI
Hazardous Waste Report Management Method Codes (!.e,, codes for hazardous waste treatment disposal, and recycling systems)
H132 12.
.
3.
I'
Designated Facility Owner or Operator: Certification of receipt of hazardous materials covered by the manifest except as noted in Item 18a . . .
Pr:ntedtTyped Name Signature . ..............Month Day Year
.1 I
EPA Form 8700-22 (Rev. 3-05) Previous editions are obsolete, GENERATOR'S INITIAL COP"
Page ,.L of
CHAIN-OF-CUSTODY RECORD I 0 s 61- - EnviroMatrfr Analytical, Inc.
ft')l'52 O(QCQ\fl1'711 V .,1Q\A'7'71 Ei4A LOG #:
I
TJ'W VIWLIU6 flV., ..fl'... fl - LPQIS £fl'..5W, ¼fl 1..J - S 1SUS UJt/a,JV Ufl
Attn: kp ¶'r (flhn 1YIj
0
#/Type
0
=
'T .
—
°
—
lu
- 00
_
.'
00
z En
I
2P
0
0r-
0
c
0
0
U
40-
2 0 0
0
x E
13
Samplers (s): 1::3rr 4. '1 (A (_U ç' (_
Address: )\ (\ 7.0
SD1'-a 1 El
Phone. Fax:
Email:
Billing Address: (1Y'i\Q
Project ID: k,
Project #: PO#:
IDS Client Sample lD
Sample
Date
Sample
Time
Sample
Matrix
Container
kk\\QC- w
uo
lf3c -
EEEEEEE EEEEEEEEEEEEEE 10
Matrix Codes: A Air, OW = Drinking Water, GW Groundwater, SW Storm Water
WW = Wastewater, S = Soil, SED = Sediment, SD = Soli&T = Tissue, 0 = Oil, L = Liquid
RELINQUI D BY DATE/TIME RECEIVED BY
Signature (244-'4.-1 1,r,ç
'1 (2' 11 C.,
print L.-( 1 nc-. Shipped By: o Courier a UPS a FedEx o USPS XClient Drop Off a Other Print -fl I 14 A a cfta 1 &Jf 'Turn-Around-Time: o Same Day X1 day o2day a3day a4day o5day a STD (7day) Company:-ç1(y\ cjr I ç' Company: 3,jJ5 'Reporting Requirements: a Fax 1'DF a Excel a Geotracker/EDF a Hard Copy a EDT Signature Signature 'Sample Disposal: )y Laboratory a 3Retum to Client: P/U or Delivery o Archive Print Print
Sample Integrity Company: Company: Correct Container(Yes)o N/A Containers Properly Preseved No N/A Signature Signature - Custody Seals Intact: Yes No Temp @ Receipt: (S" Print Print COC/Labels Agree: No N/A Isampled B)nt EMA Autosampler Company: Company:
Project/Sample Comments:
'Additional costs may apply. Please note there is a $35 minimum charge for all clients.
'EMA reserves the right to return any samples that do not match our waste profile.
NOTE: By relinquishing samples to EMA, Inc., client agrees to pay for the services requested on this COC form and any additional analyses performed on this project. Payment for services is
d
u
e
w
i
t
h
i
n
3
0
d
a
y
s
f
r
o
m
d
a
t
e
o
f
i
n
v
o
i
c
e
.
S
a
m
p
l
e
s
w
i
l
l
b
e
disposed of 7 days after report has been finalized unless otherwise noted. All work is subject to EMA's terms and conditions.
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0967
Project Name: 149570/Little-Confirmation
Notes and Definitions
S-04 The surrogate recovery for this sample is Outside of established control limits due to a sample matrix effect.
R-06 Sample dilution was necessary due to nature of the matrix.
QR-02 The RPD result exceeded the QC limits due to non-homogeneity of sample.
G-40 Gasoline Range Organics (GRO) present, but do not match gasoline fuel pattern.
D-09 Results in the diesel organics range are primarily due to overlap from a heavy oil range product.
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a thy weight basis
RPD Relative Percent Difference
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix Analytical, Inc.
Page 9 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0967
Project Name: 149570/Little-Confirmation
TPH by EPA 8015B - Quality Control
Reporting Spike Source %REC RPD
\nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 6042851
LCS (6042851-BS1) Prepared & Analyzed: 04/28/16
Diesel (C10-C28) 468 10.0 mg/kg 500 94 75-125
Surrogate: 4-Bromofiuorobenzene
LCS Dup (6042851-BSD1)
47.5 " 50.0 95 75-129
Prepared & Analyzed: 04/28/16
Diesel (C10-C28) 471 10.0 mg/kg 500 94 75-125 0.4 30
Surrogate: 4-Bromofluorobenzene
Duplicate (6042851-DUP1)
50.3 "
Source: 1600966-02
50.0 101 75-129
Prepared: 04/28/16 Analyzed: 04/29/16
Diesel (Cl0-C28)
Extended Range HC (C28-C40)
198
ND
10.0 mg/kg
10.0
195 1 30 D-09
ND 30
Surrogate: 4-Bromofiuorobenzene
Matrix Spike (6042851-MS1)
49.6 "
Source: 16D0966-02
50.0 99 75-129
Prepared & Analyzed: 04/28/16
Diesel (C10-C28) 666 10.0 mg/kg 500 195 94 75-125
Surrogate: 4-Bromofluorobenzene
Matrix Spike Dup (6042851-MSD1)
49.6 "
Source: 1600966-02
50.0 99 75-129
Prepared: 04/28/16 Analyzed: 04/29/16
Diesel (C10-C28) 673 10.0 mg/kg 500 195 96 75-125 1 30
Surrogate: 4-Bromofiuorobenzene 49.0 " 50.0 98 75-129
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix
CD
Analytical, Inc.
Page 8 of
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0967
Project Name: 149570/Little-Confirmation
TPH by EPA 8015B - Quality Control
Reporting Spike Source %REC RPD
A.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 6042836
Blank (6042836-BLK1) Prepared & Analyzed: 04/28/16
Gasoline (C6-C10) ND 0.100 mg/kg
Surrogate: 4-Bromofluorobenzene
LCS (6042836-BS1)
0.0542 " 0.0625 87 60-160
Prepared & Analyzed: 04/28/16
Gasoline (C6-C10) 0.474 0.100 mg/kg 0.500 95 70-130
Surrogate: 4-Bromofluorobenzene
LCS Dup (6042836-BSD1)
0.0507 " 0.0625 81 60-160
Prepared & Analyzed: 04/28/16
Gasoline (C6-CIO) 0.507 0.100 mg/kg 0.500 101 70-130 7 30
Surrogate: 4-Bromofluorobenzene
Duplicate (6042836-DUP1)
0.0528 "
Source: 16D0927-02
0.0625 85 60-160
Prepared & Analyzed: 04/28/16
Gasoline (C6-C10) 2.18 1.00 mg/kg 2.56 16 30 G-40
Surrogate: 4-Bromofluorobenzene
Matrix Spike (6042836-MS1)
0.0631 "
Source: 16D0967-02
0.0625 101 60-160
Prepared: 04/28/16 Analyzed: 04/29/16
Gasoline (C6-CIO) 0.460 0.100 mg/kg 0.500 ND 92 60-140
Surrogate: 4-Bromofluorobensene
Matrix Spike Dup (6042836-MSD1)
0.0714 "
Source: 16D0967-02
0.0625 114 60-160
Prepared: 04/28/16 Analyzed: 04/29/16
Gasoline (C6-CIO) 0.477 0.100 mg/kg 0.500 ND 95 60-140 30
Surrogate: 4-Bromofluorobensene
Batch 6042851
0.0693 " 0.0625 111 60-160
Blank (6042851-BLK1) Prepared & Analyzed: 04/28/16
Diesel (CIO-C28)
Extended Range HC (C28-C40)
ND
ND
10.0
10.0
mg/kg
Surrogate: 4-Bromofluorobensene 47.1 " 50.0 94 75-129
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix
(S
)Analytical, Inc.
Page 7 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0967
Project Name: 149570/Little-Confirmation
Volatile Organic Compounds by EPA Method 8260B - Quality Control
Reporting Spike Source %REC RPD
nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 6042835
Duplicate (6042835-DIJP1) Source: 16D0927-01 Prepared & Analyzed: 04/28/16
Benzene ND 2.00 ug/kg 1.70 30
Ethylbenzene 5.20 2.00 10.5 68 30 QR-02
Toluene 19.4 2.00 35.0 58 30 QR-02
m,p-Xylene 20.5 5.00 40.4 65 30 QR-02
o-Xylene 9.18 2.00 ' 18.0 65 30 QR-02
Surrogate: Dibromofluoromethane 172 " . 125 138 61-141
Surrogate: 4-Bromofluorobenzene 67.7 " 125 54 70-124 S-04
Surrogate: Toluene-d8 95.4 125 76 80-121 S-04
Matrix Spike (6042835-MS1) Source: 16D0967-02 Prepared & Analyzed: 04/28/16
Benzene 126 2.00 ug/kg 125 ND 100 77-127
Chlorobenzene 117 2.00 ' 125 ND 94 84-114
1,1-Dichloroethene 133 2.00 " 125 ND 106 61-129
Toluene 109 2.00 125 ND 87 66-139
Trichloroethene 115 2.00 125 ND 92 83-113
Surrogate: Dibromofluoromethane 145 " 125 116 61-141
Surrogate: 4-Bromofiuorobenzene 103 " 125 82 70-124
Surrogate: Toluene-d8 114 " 125 91 80-121
Matrix Spike Dup (6042835-MSD1) Source: 16D0967-02 Prepared & Analyzed: 04/28/16
Benzene 117 2.00 ug/kg 125 ND 93 77-127 7 30
Chlorobenzene 111 2.00 " 125 ND 88 84-114 6 30
1,1-Dichloroethene 121 2.00 " 125 ND 97 61-129 9 30
Toluene 100 2.00 125 ND 80 66-139 8 30
Trichloroethene 107 2.00 125 ND 86 83-113 7 30
Surrogate: Dibromofluoromethane 141 " 125 113 61-141
Surrogate: 4-Bromofluorobenzene 101 " 125 81 70-124
Surrogate: Toluene-d8 113 " 125 90 80-121
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix
(S)
Analytical, Inc.
Page 6 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0967
Project Name: 149570/Little-Confirmation
Volatile Organic Compounds by EPA Method 8260B - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 6042835
Blank (6042835-BLK1) Prepared & Analyzed: 04/28/16
Benzene ND 2.00 ug/kg
Ethylbenzene ND 2.00
Toluene ND 2.00
m,p-Xylene ND 5.00
o-Xylene ND 2.00
Surrogate: Dibromofluoromethane 129 " 125 103 61-141
Surrogate: 4-Bromofluorobenzene 121 " 125 97 70-124
Surrogate: Toluene-d8 125 " 125 100 80-121
LCS (6042835-BS1) Prepared & Analyzed: 04/28/16
Benzene 122 2.00 ug/kg 125 98 81-120
Chlorobenzene 117 2.00 ' 125 93 90-109
1,1-Dichloroethene 117 2.00 ' 125 94 67-116
Toluene 116 2.00 ' 125 93 78-112
Trichloroethene 120 2.00 " 125 96 79-108
Surrogate: Dibromofluoromethane 121 " 125 96 61-141
Surrogate: 4-Bromofluorobenzene 119 " 125 95 70-124
Surrogate: Toluene-d8 122 " 125 98 80-121
LCS Dup (6042835-BSD1) Prepared & Analyzed: 04/28/16
Benzene 120 2.00 ug/kg 125 96 81-120 2 30
Chlorobenzene 116 2.00 ' 125 92 90-109 1 30
1,1-Dichloroethene 113 2.00 125 91 67-116 3 30
Toluene 114 2.00 ' 125 91 78-112 1 30
Trichloroethene 117 2.00 " 125 94 79-108 2 30
Surrogate: Dibromofluoromethane 120 " 125 96 61-141
Surrogate: 4-Bromofluorobenzene 120 " 125 96 70-124
Surrogate: Toluene-d8 123 " 125 99 80-121
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix
(!D
Analytica1 Inc.
Page 5 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0967
Project Name: 149570/Little-Confirmation
TPH by EPA 8015B
Reporting
Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes
C - Hillside - C - W (16D0967-01) Solid Sampled: 04/28/16 11:00 Received: 04/28/16 12:55
Diesel (CIO-C28) 955 10.0 mg/kg 1 6042851 04/28/16 04/29/16 EPA 8015B D-09
Extended Range HC (C28-C40) 133 10.0 "
Surrogate: 4-Bromofluorobenzene 103% 75-129 "
Gasoline (C6-C10) 1.02 1.00 " 10 6042836 04/28/16 04/28/16 ' G40
Surrogate: 4-Bromofluorobenzene 115% 60-160 " 11 11
C - HillSide -C - E (16D0967-02) Solid Sampled: 04/28/16 11:05 Received: 04/28/16 12:55
Diesel (C1O-C28) ND 10.0 mg/kg 1 6042851 04/28/16 04/29/16 EPA 8015B
Extended Range HC (C28-C40) ND 10.0 ' " ' "
11 11
Surrogate: 4-Bromofluorobenzene 101% 75-129 " "
Gasoline (C6-C10) ND 1.00 ' 10 6042836 04/28/16 04/28/16 ' R-06
Surrogate: 4-Bromofluorobenzene 100% 60-160 " " 11
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix
C
D Analytical, Inc,
Page 4 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0967
Project Name: 149570/Little-Confirmation
Volatile Organic Compounds by EPA Method 8260B
Reporting
thalyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes
C - Hillside - C - W (16D0967-01) Solid Sampled: 04/28/16 11:00 Received: 04/28/16 12:55
Benzene ND 2.00 ug/kg 1 6042835 04/28/16 04/29/16 EPA 8260B
Ethylbenzene ND 2.00
Toluene ND 2.00
m,p-Xylene ND 5.00
o-Xylene ND 2.00
Surrogate: Dibromofluoromethane 108% 61-141 "
Surrogate: 4-Bromofluorobenzene 100% 70-124 "
Surrogate: Toluene-d8 98% 80-121 "
C - HillSide - C - E (16D0967-02) Solid Sampled: 04/28/16 11:05 Received: 04/28/16 12:55
Benzene ND 2.00 ug/kg 1 6042835 04/28/16 04/28/16 EPA 8260B
Ethylbenzene ND 2.00
Toluene ND 2.00
m,p-Xylene ND 5.00
o-Xylene ND 2.00
Surrogate: Dibromofluoromethane 111 % 61-141
Surrogate: 4-Bromofluorobenzene 92% 70-124
Surrogate: Toluene-d8 98% 80-121
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix Analytical, Inc,
Page of
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0967
Project Name: 149570/Little-Confinnation
ANALYTICAL REPORT FOR SAMPLES
Sample ID Laboratory ID Matrix Date Sampled Date Received
C - Hillside - C - W 16D0967-01 Solid 04/28/16 11:00 04/28/16 12:55
C - HillSide - C - E 16D0967-02 Solid 04/28/16 11:05 04/28/16 12:55
The results in this report apply to the samples analyzed in accordance with the chain of
custody document This analytical report must be reproduced in its entirety.
EnviroMatrix
C
D Analytical, Inc.
Page 2 of 9
EnviroMatrix Analytical, Inc.
29 April 2016
H. M. Pitt Labs, Inc.
Attn: Lee Pitt
4901 Morena Blvd., Suite 203
San Diego, CA 92117
EMA Log #: 16D0967
Project Name: 149570/Little-Confirmation
Enclosed are the results of analyses for samples received by the laboratory on 04/28/16 12:55. Samples were
analyzed pursuant to client request utilizing EPA or other ELAP approved methodologies. I certify that this
data is in compliance both technically and for completeness.
Dan Verdon
Laboratory Director
CA ELAP Certification #: 2564
4340 Viewridge Avenue, Suite A - San Diego, California 92123 - (858) 560-7717 - Fax (858) 560-7763
Analytical Chemistry Laboratory
[ b DOP D`~
CHAIN-OF-CUSTODY RECORD
PageJof
- EnviroMatrix Analytical, Inc.
410 Vi, ,ri,I,e Ave Ste A -San flinor, CA Q1T - Phone (RR\ 560-7717 - Fax (I1510 560-77G EMA LOG #: I '
Client: -\ Q\k-.- RquestedAnalysis --
Attn: (
o
,-,
V)
,
'c (N
-T
(N 00
In
a
2-CL
00
00
-
-'
00
00 I—
-
L11
0
=
z -
H
DOLLJ43
LU
C)
c
o
0 tz
0
Samplers( :Y'fl c ("kd
Address: C( r(Qn.c )k\C -2J
C1\ 2(I LU
Fax:
Email:
Billing Address: Say\Q
ProjectlD: •\-5t-\t cOv \)&:cy-,S
Project#: '\YS2..PO
ID h Client Sample ID
Sample
Date
Sample
Time
Sample
Matrix
Container
# / Type
j 1 ,cCccnDrrvi' -1-/(t1m,:0
3
4
5
6
7 -
8
9
10
Matrix Codes: A Air, OW Drinking Water, GW Groundwater, SW = Storm Water
WW = Wastewater, S = Soil. SED = Sediment, SD = Solid. T = Tissue, 0 = Oil, L = Liquid
- RELINQUI D BY DATE/TIME RECEIVED BY
Signatur/ / 6
I 1.4 5
Signalurej is lPrint 1,
Shipped By: o Courier o UPS o FedEx 0 USPS lient Drop Off 0 Other Print \ \ fg c' u 1 ic LI, 'Turn-Around-Time: o Same Day o 24 hr o 48 hr 3 day o4 day o 5 day o STD (7 day) Company: \_\-j" j \J c_b1.c Company: 'Reporting Requirements: o Fax kDF o Excel o Geotracker/EDF o Hard Copy o EDT Signature Signature
'Sample Disposal: '8a( Laboratory o 2Return to Client: P/U or Delivery o Archive Print Print
Sample Integrity Company: Company:
Correct Containers Y No N Containers Properly Preseved: No N/A Signature Signature
Custody Seals Intact: Yes No / Temp @ Receipt: 7 ( c "-,CQ- Print Print
COC/Labels Agree:(s No N/A Sampled BZIe EMA Autosampler Company: Company:
Project/Sample Comments:
'Additional costs may apply, consult a project manager for details. White- EMA Canary - Accounting Pink - Client (w/report) Gold - Client (Relinquish) 'EMA reserves the right to return any samples that do not match our waste profile.
NOTE: By relinquishing samples to EMA, Inc., client agrees to pay for the services requested on this COC form and any additional analyses performed on this project. Payment for services is due within 30 d
a
y
s
f
r
o
m
d
a
t
e
o
f
i
n
v
o
i
c
e
.
S
a
m
p
l
e
s
w
i
l
l
b
e
d
i
s
p
o
s
e
d
of after 30 days unless otherwise noted. All work is subject to EMA's terms and conditions,
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0927
Project Name: 149552/Little Consulting - Drums
Notes and Definitions
S-04 The surrogate recovery for this sample is outside of established control limits due to a sample matrix effect.
R-06 Sample dilution was necessary due to nature of the matrix.
QR-02 The RPD result exceeded the QC limits due to non-homogeneity of sample.
G-40 Gasoline Range Organics (GRO) present, but do not match gasoline fuel pattern.
D-09 Results in the diesel organics range are primarily due to overlap from a heavy oil range product.
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
thy Sample results reported on a dry weight basis
RPD Relative Percent Difference
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix
(S
) Anaiyticai, Inc.
Page 9 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0927
Project Name: 149552/Little Consulting - Drums
TPH by EPA 8015B - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 6042851
LCS (6042851-BSI) Prepared & Analyzed: 04/28/16
Diesel (CIO-C28) 468 10.0 mg/kg 500 94 75-125
Surrogate: 4-Bromofluorobenzene
LCS Dup (6042851-BSD1)
47.5 " 50.0 95 75-129
Prepared & Analyzed: 04/28/16
Diesel (C10-C28) 471 10.0 mg/kg 500 94 75-125 0.4 30
Surrogate: 4-Bromofluorobenzene
Duplicate (6042851-DUP1)
50.3
Source: 16D0966-02
11 50.0 101 75-129
Prepared: 04/28/16 Analyzed: 04/29/16
Diesel (C1O-C28)
Extended Range HC (C28-C40)
198
NT)
10.0 mg/kg
10.0 '
195 1 30 D-09
ND 30
Surrogate: 4-Bromofluorobenzene
Matrix Spike (6042851-MS1)
49.6 "
Source: 16D0966-02
50.0 99 75-129
Prepared & Analyzed: 04/28/16
Diesel (CIO-C28) 666 10.0 mg/kg 500 195 94 75-125
Surrogate: 4-Bromofluorobenzene
Matrix Spike Dup (6042851-MSD1)
49.6 "
Source: 16D0966-02
50.0 99 75-129
Prepared: 04/28/16 Analyzed: 04/29/16
Diesel (C10-C28) 673 10.0 mg/kg 500 195 96 75-125 1 30
Surrogate: 4-Bromofluorobenzene 49.0 " 50.0 98 75-129
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix
C
D Analytica1, Inc
Page 8 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0927
Project Name: 149552/Little Consulting - Drums
TPH by EPA 8015B - Quality Control
Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 6042836
Blank (6042836-BLK1) Prepared & Analyzed: 04/28/16
Gasoline (C6-C1O) ND 0.100 mg/kg
Surrogate: 4-Bromofluorobenzene
LCS (6042836-BS1)
0.0542 ' 0.0625 87 60-160
Prepared & Analyzed: 04/28/16
Gasoline (C6-C10) 0.474 0.100 mg/kg 0.500 95 70-130
Surrogate: 4-Bromofluorobenzene
LCS Dup (6042836-BSD1)
0.0507 " 0.0625 81 60-160
Prepared & Analyzed: 04/28/16
Gasoline (C6-C10) 0.507 0.100 mg/kg 0.500 101 70-130 7 30
Surrogate: 4-Bromofluorobenzene
Duplicate (6042836-DUP1)
0.0528 "
Source: 16D0927-02
0.0625 85 60-160
Prepared & Analyzed: 04/28/16
Gasoline (C6-C10) 2.18 1.00 mg/kg 2.56 16 30 G40
Surrogate: 4-Bromofluorobenzene
Matrix Spike (6042836-MS1)
0.0631 "
Source: 16D0967-02
0.0625 101 60-160
Prepared: 04/28/16 Analyzed: 04/29/16
Gasoline (C6-C1O) 0.460 0.100 mg/kg 0.500 ND 92 60-140
Surrogate: 4-Bromofluorobenzene
Matrix Spike Dup (6042836-MSD1)
0.0714 "
Source: 16D0967-02
0.0625 114 60-160
Prepared: 04/28/16 Analyzed: 04/29/16
Gasoline (C6-CIO) 0.477 0.100 mg/kg 0.500 ND 95 60-140 30
Surrogate: 4-Bromofluorobenzene
Batch 6042851
0.0693 " 0.0625 111 60-160
Blank (6042851-BLK1) Prepared & Analyzed: 04/28/16
Diesel (CIO-C28)
Extended Range HC (C28-C40)
ND
ND
10.0
10.0
mg/kg
11
Surrogate: 4-Bromofiuorobenzene 47.1 " 50.0 94 75-129
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix
(
D Analytical, Inc.
Page 7 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0927
Project Name: 149552/Little Consulting -Drums
Volatile Organic Compounds by EPA Method 8260B - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 6042835
Duplicate (6042835-DUP1) Source: 16D0927-01 Prepared & Analyzed: 04/28/16
Benzene ND 2.00 ug/kg 1.70 30
Ethylbenzene 5.20 2.00 10.5 68 30 QR02
Toluene 19.4 2.00 35.0 58 30 QR02
m,p-Xylene 20.5 5.00 ' 40.4 65 30 QR02
o-Xylene 9.18 2.00 18.0 65 30 QR02
Surrogate. Dibromofluoromethane 172 " 125 138 61-141
Surrogate: 4-Bromofluorobenzene 67.7 " 125 54 70-124 S-04
Surrogate: Toluene-d8 95.4 " 125 76 80-121 S-04
Matrix Spike (6042835-MS1) Source: 1600967-02 Prepared & Analyzed: 04/28/16
Benzene 126 2.00 ug/kg 125 ND 100 77-127
Chlorobenzene 117 2.00 125 ND 94 84-114
1,1-Dichloroethene 133 2.00 ' 125 ND 106 61-129
Toluene 109 2.00 125 ND 87 66-139
Trichloroethene 115 2.00 125 ND 92 83-113
Surrogate: Dibromofluoromethane 145 " 125 116 61-141
Surrogate: 4-Bromofluorobenzene 103 " 125 82 70-124
Surrogate: Toluene-d8 114 " 125 91 80-121
Matrix Spike Dup (6042835-MSD1) Source: 1600967-02 Prepared & Analyzed: 04/28/16
Benzene 117 2.00 ug/kg 125 ND 93 77-127 7 30
Chlorobenzene 111 2.00 125 ND 88 84-114 6 30,
1,1-Dichloroethene 121 2.00 ' 125 ND 97 61-129 9 30
Toluene 100 2.00 ' 125 ND 80 66-139 8 30
Trichloroethene 107 2.00 125 ND 86 83-113 7 30
Surrogate: Dibromofluoromethane 141 " 125 113 61-141
Surrogate: 4-Bromofluorobenzene 101 " 125 81 70-124
Surrogate: Toluene-d8 113 " 125 90 80-121
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix Analytical, Inc.
Page 6 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0927
Project Name: 149552/Little Consulting - Drums
Volatile Organic Compounds by EPA Method 8260B - Quality Control
Reporting Spike Source %REC RPD \nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 6042835
Blank (6042835-BLK1) Prepared & Analyzed: 04/28/16
Benzene ND 2.00 ug/kg
Ethylbenzene ND 2.00
Toluene ND 2.00
m,p-Xylene ND 5.00
o-Xylene ND 2.00
Surrogate: Dibromofluoromethane 129 " 125 103 61-141
Surrogate: 4-Bromofluorobenzene 121 " 125 97 70-124
Surrogate: Toluene-d8 125 " 125 100 80-121
LCS (6042835-BS1) Prepared & Analyzed: 04/28/16
Benzene 122 2.00 ug/kg 125 98 81-120
Chlorobenzene 117 2.00 ' 125 93 90-109
l,1-Dichloroethene 117 2.00 ' 125 94 67-116
Toluene 116 2.00 125 93 78-112
Trichloroethene 120 2.00 125 96 79-108
Surrogate: Dibromofluoromethane 121 " 125 96 61-141
Surrogate: 4-Bromofluorobenzene 119 " 125 95 70-124
Surrogate: Toluene-d8 122 " 125 98 80-121
LCS Dup (6042835-BSD1) Prepared & Analyzed: 04/28/16
Benzene 120 2.00 ug/kg 125 96 81-120 2 30
Chlorobenzene 116 2.00 " 125 92 90-109 1 30
1,1-Dichloroethene 113 2.00 ' 125 91 67-116 3 30
Toluene 114 2.00 125 91 78-112 1 30
Trichloroethene 117 2.00 ' 125 94 79-108 2 30
Surrogate: Dibromofluoromethane 120 " 125 96 61-141
Surrogate: 4-Bromofluorobenzene 120 " 125 96 70-124
Surrogate: Toluene-d8 123 " 125 99 80-121
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix Analytical, Inc.
Page 5 of
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0927
Project Name: 149552/Little Consulting - Drums
TPH by EPA 8015B
Re orting
Analyte Result &mit Units Dilution Batch Prepared Analyzed Method Notes
55 Gallon Drum I (16130927-01) Soil Sampled: 04/27/16 11:00 Received: 04/27/16 14:15
Diesel (C10-C28) 34400 1250 mg/kg 25 6042851 04/28/16 04/29/16 EPA 8015B D-09
Extended Range HC (C28-C40) 8890 1250 1
1'
Surrogate: 4-Bromofluorobenzene 101% 75-129 " " 04/29/16
Gasoline (C6-C10) 1.37 1.00 ' 10 6042836 04/28/16 04/28/16 G-40
Surrogate: 4-Bromofluorobenzene 90% 60-160 "
55 Gallon Drum 2 (16D0927-02) Soil Sampled: 04/27/16 11:05 Received: 04/27/16 14:15
Diesel (C10-C28) 15500 100 mg/kg 10 6042851 04/28/16 04/29/16 EPA 8015B D-09
Extended Range HC (C28-C40) 2940 100 ' ' '
11 11 11
Surrogate: 4-Bromofluorobenzene 101% 75-129 " " 04/29/16
Gasoline (C6-CIO) 2.56 1.00 10 6042836 04/28/16 04/28/16 ' G-40
Surrogate: 4-Bromofluorobenzene 111 % 60-160 " " 11
The results in this report apply to the samples analyzed in accordance with the chain of
custody document This analytical report must be reproduced in its entirety.
EnviroMatrix Analytical, Inc.
CD
Page 4 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0927
Project Name: 149552/Little Consulting - Drums
Volatile Organic Compounds by EPA Method 8260B
Reporting
Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes
55 Gallon Drum 1 (16D0927-01) Soil Sampled: 04/27/16 11:00 Received: 04/27/16 14:15 R-06
Benzene ND 8.00 ug/kg 4 6042835 04/28/16 04/29/16 EPA 8260B
Ethylbenzene 10.5 8.00
Toluene 35.0 8.00
m,p-Xylene 40.4 20.0
o-Xylene
- 18.0 8.00
Surrogate: Dibromofluoromethane 129% 61-141 "
Surrogate: 4-Bromofluorobenzene 55% 70-124 " 0 ' ' S-04
Surrogate: Toluene-d8 78% 80-121 fi' fi' 'fi ' S-04
55 Gallon Drum 2 (16D0927-02) Soil Sampled: 04/27/16 11:05 Received: 04/27/16 14:15 R-06
Benzene ND 8.00 ug/kg 4 6042835 04/28/16 04/29/16 EPA 8260B
Ethylbenzene 14.5 8.00
Toluene 62.1 8.00
m,p-Xylene 55.8 20.0 '
o-Xylene 26.1 8.00
Surrogate: Dibromofluoromethane 127% 61-141
Surrogate: 4-Bromofluorobenzene 64% 70-124 " 'fi " ' S-04
Surrogate: Toluene-d8 81% 80-121
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix Analytical, Inc,
Page 3 of 9
Client Name: H. M. Pitt Labs, Inc. EMA Log #: 16D0927
Project Name: 149552/Little Consulting - Drums
ANALYTICAL REPORT FOR SAMPLES
Sample ID Laboratory ID Matrix Date Sampled Date Received
55 Gallon Drum 1 16D0927-01 Soil 04/27/16 11:00 04/27/16 14:15
55 Gallon Drum 2 16D0927-02 Soil 04/27/16 11:05 04/27/16 14:15
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
EnviroMatrix(S)Analytical, Inc.
Page 2 of 9
EnviroMatrix Analytical, Inc.
29 April 2016
H. M. Pitt Labs, Inc.
Attn: Lee Pitt
4901 Morena Blvd., Suite 203
San Diego, CA 92117
EMA Log #: 16D0927
Project Name: 149552/Little Consulting - Drums
Enclosed are the results of analyses for samples received by the laboratory on 04/27/16 14:15. Samples were,
analyzed pursuant to client request utilizing EPA or other ELAP approved methodologies. I certify that this
data is in compliance both technically and for completeness.
Dan Verdon
Laboratory Director
CA ELAP Certification #: 2564
4340 Viewridge Avenue, Suite A - San Diego, California 92123 - (858) 560-7717 - Fax (858) 560-7763
Analytical Chemistry Laboratory