HomeMy WebLinkAbout38022; Pine Park; Contaminated Soil Disposal Madison Street; 2002-07-03Geotechnical and Environmental Sciences Consultants
July 3, 2002
ProjectNo. 104567002
Mr. Keith Beverly
City of Carlsbad
1200 Carlsbad Village Drive
Carlsbad, Cahfomia 92008
Subject: Report of Chemical Disposal and Excavation of Contaminated Soil
3354 and 3366 Madison Street
Carlsbad, Cahfomia
Reference: "Phase I Environmental Site Assessment Update and Hazardous Building Materi-
als Survey, 3354 and 3366 Madison Street, Carlsbad, Califomia," prepared by
Nmyo & Moore, dated Febmary 4, 2002.
Dear Mr. Beverly:
This letter report documents the disposal of miscellaneous abandoned cheraicals and the excava-
tion and disposal of petroleum hydrocarbon stained soiT from the property located at 3354 and
3366 Madison Street m Carlsbad, Califomia (site, Figure 1). Work was conducted in general ac-
cordance with our proposal dated Febmary 22, 2002, (revised March 6, 2002) and your
authorization to proceed.
BACKGROUND
The findmgs of Nuiyo & Moore's referenced Phase I Environmental Site Assessment Update
(ESAU) for the subject site stated the following:
"Abandoned waste oil and antifreeze containers were observed adjacent to the northeast
wall ofthe garage structure during the site reconnaissance. An approximately 10-foot by
12-foot stained area was noted in the vicinity of the materials. An approximately 3-foot by
6-foot stained area also was noted in the unpaved driveway between the two residences.
Prior to building demolition activities, the abandoned materials should be removed and
properly disposed. The stained soil should be excavated, and soil samples should be
collected to confirm the complete removal of contaminated soils."
5710 Ruffin Road " San Diego, California 92123 » Phone (858) 576-J 000 •• Fax (858] 576-9600
San Diego ° Irvine ° Ontario • Los Angeles • Oakland » Las Vegas • Salt Lake City ° Phoenix
City of Carlsbad July 3, 2002
3354 and 3366 Madison Street, Carlsbad Project No. 104567002
OBJECTIVES
The objective of the work was to remove and properly dispose of the abandoned chemicals, as
weir as thc stained soil in the noted areas.
CHEMICAL DISPOSAL ACTIVITIES
On April 10, 2002, Ninyo & Moore contracted EFR Environmental Services Inc. (EFR) to col-
lect and package the abandoned chemicals located in the exterior garage area ofthe subject site.
The packaged materials included one, 5 5-gallon container of used oil fihers and oily debris, one,
55-gallon container of oily water, and one cubic yard box of miscellaneous materials, mcluding
adhesives and paint. The waste containers were classified as non-hazardous waste, and were
loaded and transported by EFR on May 15, 2002, to the Dome Rock hidustries facility in
Quartzsite, Arizona for recycling/disposal. A copy of the Non-Hazardous Waste Manifest has
been included in Attachment 1.
EXCAVATION ACTIVITIES
On April 11, 2002 , Ninyo & Moore contracted EFR to excavate the stained soil in the driveway
and the exterior garage area ofthe site. Prior to excavation activities, the City of Carisbad con-
firmed that the utilities at the site had been abandoned.
EFR utilized a backhoe to excavate an area measuring approximately 12-feet-long by 7-feet-
wide, to a depth of approximately 3.5 feet below ground surface (bgs), m the exterior garage
area. The soil removal activities were advanced to a depth and extent where no stained or odor-
ous soil was noted on the floor or sidewalls of the excavation. One confirmation soil sample was
collected from each sidewall (NSW-02, ESW-02, SSW-02, and WSW-02), and one soil sample
was collected from the floor ofthe excavation (EB-03.5) (Figure 2). EFR removed an approxi-
mately 5-foot-long by 7-foot-wide area of stained soil in the driveway of the site, to a depth of
one foot bgs. One confirmation soil sample was collected from the floor of the driveway area
excavation (DWB-01) and one soil sample was collected from the stockpiled spoils (SPl) for
disposal characterization.
4567002cxcavadon letter.doc
City of Carlsbad
3354 and 3366 Madison Street, Carlsbad
July 3, 2002
Project No. 104567002
The soil samples were submitted to Sierra Analytical Laboratory in Laguna Hills, Califomia. The
confirmation soil samples were analyzed for total petroleum hydrocarbons, extended range hy^
drocarboris (TPHe) by United States Environmental Protection Agency (USEPA) method
number 8015 Modified. Concentrations of TPHe were detected in samples SSW-02 and EB-03.5
at 780 and 543 milligrams per kilogram (mg/kg), respectively. Laboratory reports have been in-
cluded as Attachment 2. A summary of the confirmation soil sample laboratory results is
contained in Table 1.
Table 1 - Summary of Confirmation Soil Sample Laboratory Results
Boring
Location Sample No. Depth
(feet)
TPHe
(mg/kg)
Garage excavation - floor EB-03.5 3.5 543
Garage excavation - north sidewall NSW-02 2 ND
Garage excavation - east sidewall .ESW-02 •.. 2 • . : ND .
Garage excavation - south sidewall ..V/ SSW-02,. ;;: • •/•;..2-:;
Garage excavation - west sidewall WSW-02 2 ND
Driveway excavation - floor DWB-01 1 ND
Notes:
feet - feet below ground surface (bgs)
TPHe - Total petroleum hydrocarbons, extended range hydrocarbons C7-C36 analyzed in general accordance with
USEPA method 8015M
mg/kg - milligrams per kilogram
ND - No detectable concentration above the laboratory detection limit
The soil sample analytical results indicate that the extent of the remaining petroleum hydrocar-
bon impacted soil has not been dehneated in the vertical and southerly directions. The
concentrations of TPHe detected in the confirmation soil samples were reported in the general
carbon range of C24 through C32, indicating a heavy petroleimi hydrocarbon such as waste motor
oil. It should also be noted that the soil sample with the highest TPHe concentration (SSW-02)
and the stockpile soil sample (SP-1) were additionally analyzed for volatile organic compoimds
(VOCs) by USEPA test method 8260B, and for Califomia Title 22 metals by USEPA test meth-
ods 601 OB/7471. Neither VOCs nor elevated levels of metals were detected in either ofthe soil
samples.
4567002excavalion letter.doc
City of Carlsbad July 3, 2002
3354 and 3366 Madison Street, Carlsbad Project No. 104567002
EXCAVATION ACTIVITIES
Following the excavation activities, the excavated area was backfilled with surface material
scraped from the surrounding yard area and compacted with the back hoe. Soil generated from
the excavation activities was stored at the site in a secure, 20-cubic-yard transport bin. Based on
the laboratory analyses ofthe soil stockpile sample, the soil was classified as non-hazardous soil.
On May 15, 2002, approximately 14.4 tons of non-hazardous soil was loaded and transported to
Dome Rock Industries. The soil was received at the facility on May 20, 2002. A copy of the
Non-Hazardous Waste Manifest is included in Attachment 1.
DISCUSSION AND CONCLUSIONS
The soil sample analytical results indicate that petroleum hydrocarbon contammated soil remains
below and to the south ofthe garage area excavation. The concentrations of TPHe defected in the
confirmation soil samples were reported in the general carbon range of C24 through C32, mdicat-
ing a heavy petroleum hydrocarbon such as waste motor oil.
Our review of a groundwater monitoring report for a nearby property indicated that the static
groundwater level in the vicinity of the site is approximately 14 feet below ground surface, and
the direction of groundwater flow is to the west-northwest. Based on the fact that heavy petro-
leum hydrocarbons such as those detected at the site do not typically move rapidly through soil,
and because the former residential use ofthe site suggests that relatively small amounts of these
constituents were stored in this area, there is low likelihood that groundwater has been signifi-
cantly impacted by this release of heavy petroleum hydrocarbons. Furthermore, the site is located
west of Interstate 5, which is an area where the Regional Water Quality Control Board has ex-
cepted groundwater from beneficial use designation.
There are no regulatory standards for petroleum hydrocarbon cleanup levels. Regulatory agen-
cies typically set cleanup standards on a case-by-case basis based on a number of variables
including soil lithology, depth to groundwater, chemical constituents, concentrations, risk to
health and the environment, and/or land use. Based on the chemical constituent detected (i.e.,
heavy petroleum hydrocarbons), the fact that neither VOCs nor elevated levels of metals were
4567002cxcavation letter.doc
City of Carlsbad July 3, 2002
3354 and 3366 Madison Street, Carlsbad Project No. 104567002
detected in the two samples analyzed for these constituents, the depth to groundwater (estimated
at 14 feet bgs), and the non-beneficial use groundwater designation, it is our opinion that there is
a low likelihood that these cohcentrations would be of concem to a regulatory agency based on
current site use. However, it should be noted that if the remaining contaminated soil is excavated
and exported from the site, it would be considered a waste by the Regional Water Quality Con-
trol Board and accepting disposal facility.
LIMITATIONS
The environmental services described m this report have been conducted in general accordance
with current regulatory guidelines and the standard-of-care exercised by environmental consuh-
ants performing similar work in the project area. No warranty, expressed or imphed, is made
regarding the professional opinions presented in this report. Please note that this study did not
include an evaluation of geotechnical conditions or potential geologic hazards.
This document is intended to be used only in its entkety. No portion ofthe document, by itself, is
designed to completely represent any aspect of the project described herein. Ninyo & Moore
should be contacted if the reader requnes any additional information or has questions regarding
the content, interpretations presented, or completeness ofthis document.
Our findings and opinions are based on an analysis of the observed site conditions and the refer-
enced literature. It should be understood that the condhions of a site could change with time as a
resuh of natural processes or the activities of man at the subject site or nearby sites. In addition,
changes to the applicable laws, regulations, codes, and standards of practice may occur due to
govemment action or the broadening of knowledge. The findmgs of this report may, therefore, be
invalidated over time, in part or in whole, by changes over which Nmyo & Moore has no control.
This report is intended exclusively for use by the chent. Any use or reuse of the findings, conclu-
sions, and/or recommendations ofthis report by parties other than the chent is undertaken at said
parties' sole risk.
4567002cxcavation letter.doc
City of Carlsbad July 3, 2002
3354 and 3366 Madison Sti-eet, Carisbad Project No. 104567002
We appreciate the opportunity to be of service on this project. If you have any questions or
coniments regarding this report, please call the undersigjied at your convenience.
Sincerely,
NINYO & MOORE
Travis L. Stravasnik Stephan A. Beck, C.E.G., HG., R.E.A. H
Project Environmental Scientist Manager, Environmental Sciences Division
TLS/SB/kmf
Attachments: Figure 1 - Site Location Map
Figure 2 - Soil Sample Location Map
Attachment 1 - Laboratory Analytical Results and Chain-of-Custody Records
Attachment 2 - Non-Hazardous Waste Manifests
Distribution: (2) Addressee
4567(X)2cxcavaion letter.doc
REFERENCE: 2001 THOMAS GUIDE FOR SAN DIEGO COUNTY, STREET GUIDE AND DIRECTORY
SITE LOCATION MAP
3354 AND 3366 MADISON STREET
CARLSBAD, CALIFORNIA
PROJECT NO.
104567002
DATE
7/02 C FIGURE
1
r
MADISON STREET
\
0 NSW-02 \
(ND) \ ^ LIMIT OF EXCAVATION
V ESW-02
•^(ND)
LEGEND
^ SSW-02 Anproximate location of soil sample and TPH-e concentration (mg/kg) (800)
scale
10
feet J
^in I/O &yy\Diir e_
SOIL SAMPLE LOCATION MAP
3354 AND 3366 MADISON STREET
CARLSBAD, CALIFORNIA
V
r PROJECT NO. DATE A
^ 104567002 7/02 J
FIGURE
Industries, Inc.
Phone: (928)927-7688 '' 3125 West Dome Rock Road
Fax: (928) 927-7689 :. / f , • ; V P
E-Mail: iriiKizniatuffiiUs.iiei'; . • Quartzsite, Arizona 85359-3063 ,
Dear Customer,
We would like to thank you for choosing Dome Rock Industries, Inc. as your
recycler for your Non-RCRA Hazardous Waste.
Attached, please find your Non-RCRA Hazardous Waste Manifest(s) used in
the transportation of the waste from your facility to ours.
If you should have any questions regarding this manifest, please do not
hesitate to contact me.
Sincerely,
Jerry R.Afarrett
Plant Manager A Compliance Director
IState of California—Environmental Protection Agency
Form Approved OMft No. 2050-0039 (Expires 9-30-99)
Please prinf br type. ' Form designed for use on elite 112-pitcb) typev/riter.
See Instructions on back of page 6. Department of Toxic Substances Control
Sacramento, California
UNIFORM HAZARDOUS
WASTE MANIFEST
1. Generator's US EPA ID No. Manifest Document No.
C| A| C|0|G| 2| 5| .51 1| 9| 9| 2| 2 | 0 7 5 12 ofl
Information in tfie shaded areas
is not required by Federal law.
3. Generator's Name and Moiling Address
City of Carlsbad
3354-3360 Madison Street, Carlsbad, CA 92008
4. Generator's Phone ( 85$ 5f6-1000 Cotitact t Travls Stravasnik
A. State Manifest Document Number 21860155
B. State Generator's ID
6. US EPA ID Number 5. Transporter 1 Company Name
... , EFR Enyironfflental Services, Ing.^ ^ 2,.
C. State Transporter's ID [Reserved.]
D. Trqrispprter's Plione '.^ ^ j 9 ) 9f>6-2770
7. Transporter 2 Compqriy Nome .8. .US EPA ID Number E. estate Transporter's ID fReserved. 1
F. Transporter's Phone . *.
9. Designated Facility Name and Site Address
Dome Rock Industries, Inc.
3125 W. Dome Rock Road
Quartzsite, A2 85346
10. us EPA ID Number G. State Facility's ID
H. Facility's Phone
A|Z|R|0|0|0|0| 31 51 9| 1| 5 928-^27-7688
11. us DOT Description (including Proper Shipping Name, Hazard Class, and ID Number) 1 2. Containers
No. Type
13. Total
Quantity
14. Unit
Wt/Vol I. Waste Number
Non-RCRA Hazardous Waste Liquid G
State. 134
0 mov\0[}^ EPA/Other
.Non-RCRA
Non-RCR/\ Hazardous Waste Solid
State 352
OQ\( 0 \(^G^\L\c\^ EPA/othe^ion-RGRA
Non-RCRA Hazardous Waste Solid state 281/291
C \ f-O\O\^\0\o EPA/otheMon-RCRA:
State
EPA/Other
J. Additioridi Descriptions for Materials Listed Above " •'
• 11a: Acceptance#/ff4>^-'7i32j3
' 1l'b. Acceptance^/^^^^^(JOZ.
11c. Acceptance*.
(Oily Water)
(Oily Debris,)
(Adh,8siye.s, Latex, Tar)
K. Handling Codes for Wdstes Listed Above
° O]
15. Special Handling Instructions and Additional Information
A3.WAYS W.^ .APPROPRIATE PPE AND USE SAFE E\NDLING METHODS
24 HOUR EMERGENCY NUMBER (SOO) 244-1202 *EFR* or (800) 424-9300 ^CHE^flREC*
Please faail C/0 Ninvo & Moore-5710 Ruffin Pvd., San Diego, GA 92123
1 6. GENERATOR'S CERTIFICATION: I fiereby declare tfiat the contents of tfiis consignment are fully and accurafelv described above by proper shipping nome and are classified, packed,
marked, and labeled, and are in ail respects in proper condition for transport by fiigtiway according to applicable international and notional government regulations.
If I am a targe quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically
practicable and that I have selected the practicable method oT treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health
and the environment; OR, if I am a smoll quantity generator, I have mode a good faith effort lo minimize my waste generation and select the best waste management method that is
available to me and that I can afford.
17. Transporter 1 Acknowledgement of Receipt of Materials
Prinfed/t^^tf^ Ncyne X^^'J
18. Transporter 2 Acknowledgement of Receipt of Materials
Month Day Year
^15 1/ i 5io.r^
Printed/Typed Name Signature Month Day Year
I
19. Discrepancy Indication Space
20. Facility Owner or Operator Certification of receipt of hazardous materials covered by this mgnifajtexcept as noted in Item 1 9.
Printed/Typed Nome --^O /
DO NOT
X Month_, Day Year
0^ 9 3 vA-
DTSC 8022A (1/99)
EPA 8700-22
ELOW Jk^i UNE.
Yellov^: TSDF SENDS THIS COPY TO GENERATOR WIPrilN 30 DAYS.
(Generators v^ho submit hazardous waste for transport out-of-state,
produce completed copy of this copy and send to DTSC within 30 days.)
Industries, Inc.
Phone: (928) 927-7688 3125 West Dome Rock Road
Fax: (928) 927-7689 PO Box 3063
- E-Mail: irihazmanfS tds.ner Quartzsite, Arizona 85359-3063
Dear Customer,
We would like to thank you for choosing Dome Rock Industries, Inc. as your
recycler for your Non-Hazardous Waste.
Attached, please find your Non-Hazardous Waste Manifest (s) used in the
transportation of the waste from your facility to ours.
Ifypu should have any questions regarding this manifest, please do not
hesitate to contact me.
Sincerely,
( Jerry R. Jarrett J^rry R. Jarrett
Plant Manager A Compliance Director
I
I
i
iState of California—Environmental Protection Agency
Form Approved OMB No. 2050-0039 (Expires 9-30-99)
Please print'or type. Form designed for use on elite {12'pitc
See Instructions on back of ooge 6. Department of Toxic Substances Control
Sacramento, California
i
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
UNIFORM HAZARDOUS
WASTE MANIFEST
,. Generator's US EPA ID No. Manifest Document No,
C|A|C|O|0|2|5|5| 1|9|9|2|2 |0
3. Generator's Name arid Mailing Address
• City of Carlsbad ,
3354-3360 Madison Street, Carlsbad, CA 92008
4. Generator's Phone 1 858 576-1000 Contact: Travjs stravasnik
6. US EPA ID Number 5. Transporter 1 Company Name
EFR Enviroarnental..Services, ^^g-^ 0 0 0 0|1|1|2|0|5
7.. Transporter 2;Company Name Q: US EPA ID Number .
9 Designated Facility Name and Site Address
Dome Rock Industries, Inc.
312.5 W, Dome Rock Road
Quartzsite, AZ 85346
10. us EPA ID Number
5 13
2. Page 1
ofl
Information in the shaded areas
is not required by Federal law.
A. State Manifest Document Number 21860156
B. State Generator's ID
r I I I I C. state Transporter's ID I Reserved.!
D.. Transporter's Phone .( 61 9 ) . 956-2770
E. Stale,Transporter's.ID [Reserved.]
F. Transporter's Phone
G. State Facility's ID
|A|Z|R|0|0|0|0|3|5|.9i1|5
H. Facility's Phone
928-927-7688:
11. us DOT Description (including Proper Shipping Nome, Hazard Class, and ID Number)
'Non-RCRA Hazardous Waste Solid
12. Containers
No.
J- ^''•'•f5i"|'f"Xc^ce^tan^^^ (Oi 1 Cont. Soil ;
^/mA!s^/p4
Type
h\7
13. Total
Quantity
o\o\o\'X\o
14. Unit
Wl/Vol I. Waste Number
State 3bli -
EPA/Othe 'Ron-RCRA
State
EPA/Other
State
EPA/Other
Stale
EPA/Other
K , Handling Cades'for Wastes Listed Above
:b.-' ';V I.?. " ol
15 Special Handling Instructions and Additional Information
ALWAYS WEAPv APPROPRIATE PPE AND USE SAFE Hi'^NDLING METHODS ^ ^ _
24 HOUR EMERGENCY NUMBER (800) 244-1202 *£FFlV; or t800} 424-9300 *CH.i'..TrR£.;_.
Piease mai.! C/0 Ninyo & Moore-5710 Raff in Rd. > San Diego, CA 92123
16 GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurotelv described above by proper shipping name and P°'^'<^'''
morkeTond labeled, and are in all respects in proper condition for transportty highway according to applicable internot.onal and national government regulohons.
available to me and tfiat I can afford.
17^ Transporter 1 Acknowledgement of Receipt of Materials ^ ; y ..• yy ^
"m'lr^ i^s A;^/ rxv&iMA^^.?Axy-
. Transporter X^cknowledg
Month
Mil
Day Year
i\^\oX\
lement of Receipt of Materials
Printed/Typed Name Signature Month Day Year
1 9. Discrepancy Indication Spoce
20. Facility Owner or Operator Certificotion of receipt of hazardous materials.covared by this monifasfexcept as noted in Item 19
Printed/Typed Name / Month Day ^^'^
0\f \c^^P \^rrL
DTSC 8022A (1/99)
EPA 8700—22
BELOW/THIS LINE.
Yellow: TSDF SENDS THIS COPY TO GENERATOR WITHIN 30 DAYS.
(Generators who submit hazardous waste for transport out-of-state,
produce completed copy of this copy and send to DTSC within 30 days.)
A
SIERRA
ANALYTICAL
Date: 04/25/02
Ninyo & Moore
5710 Ruffin Road
San Diego, CA. 92123
Attention: Mr. Travis Stravasnik
Client Project Number:
Date Sampled:
Date Samples Received:
Sierra Project No.:
104567002/3354 & 3366
Madison St, Carlsbad
04/11/02
04/11/02
0204-213
Attached are the results ofthe chemo-physical analysis ofthe sample(s) from the project identified above.
The samples were received by Sierra Laboratones, Inc. with a chain of custody record attached or
completed at the submittal of the samples.
The analysis were perfbimed according to the prescribed method as outlined by EPA, Standard
•'Methods,,:aridA.S;T.M. • "^^^ ' y ••
The remaining portions ofthe samples will be disposed of within 30 days from the date ofthis report.
If you require additional retaining time, please advise us.
A/
Richard K. Forsyth
Laboratory Director
Reviewed
n,is report is applicable only to the sample received by the laboraU>ry. Tl,e liability ofthe laboratory is h„,„ed to the antoun. pa,d for ,b,s report, l l„s report ,s tor the
exclusive t.e of U,e client to whom it is addressed and upon the condtdon U,at the client assumes all.Hab.Hty for the further d.stribut.ou ofthe report or „.s contents.
26052 MERIT CIRCLE SUITE 105, LAGUNA HILLS, CALIFORNIA 92653
TELEPHONE: (949) 348-9389 FAX: (949) 348-9115
E-MAIL: SIERFVI.LABS@EARTHLINK.NET
SIERRA ANALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA. 92123
Sierra Project No.:
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213 Analyst:
104567002 / 3354 & 3366 Madison St, Carlsbad
Soil Report Date:
2320
04/11/02
04/11/02
04/16/02
04/16/02
GW
04/17/02
Total Petroleum Hydrocarbons (TPH) by GC/FID
Preparation Method: Sonication Extraction (EPA Metiiod 3550)
EPA Metiiod 8015B Extractable Organics (C7-C36)
Sierra Sample No.: Client Sample No.: TPH Concentration
(mg/Kg)
Dilution
Factor
Surrogate %
Recovery
PQL
(mg/Kg)
7560 NSW-02 ND 1 103 5.0
7561 ESW-02 ND 1 98 5.0
7563 WSW-02 ND 1 108 5.0
7565 DWB-01 ND 1 112 5.0
7566 SPl 200 1 122 5.0
1 Quality Assurance / Quality Control Data
lor Reference No.: 020313-Blank 1
Unalytes: LCS
% Rec.
LCS QC
Limits
Spike
% Rec.
Spilte Dup.
% Rec.
Spike
QC Limits RPD RPD 1
QC Limits 1
piesel 86 80-120 84 80 50- 150 4.9 0-30 1
ND means Not Detected
Reporting Limit (RL) = Practical Quantitation Limit (PQL) x Dilution Factor
SIERRA ANALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA 9213
Sierra Project No.:
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213 Analyst:
104567002 / 3354 & 3366 Madison St, Carlsbad
Soil Report Date:
2320
04/11/02
04/11/02
04/16/02
04/16/02
GW
04/30/02
Total Petroleum Hydrocarbons Carbon Range Analysis (GC/FID)
Preparation Method: Sonication Extraction (EPA Method 3550)
Analysis Method: EPA Method 8015B
CHent Sample No.;
Sierra Sample No.
SSW-02
7562
EB-03.5
7564
Practical
Quantitation
Limit
Analytes:
HC<C8
C8 < HC < C9
C9<HC<C10
C10<HC<C11
CM <HC < GI2
C12<HC^C14
C14<HC<C16
C16<HC<C18
C18<HC<C20
C20 < HC < C24
C24<HC<C28
C28 < HC < C32
HC > C32
Total
ND
ND
ND
ND
ND
ND
ND
ND
ND
120
460
200
ND
780
ND
ND
ND
ND
ND
ND
1.2
ND
1.5
47
220
220
53
543
1.0
1.0
1.0
1.0
1.0
1.0 .
^ i:o'
1.0
1.0
1.0
1.0
1.0
1.0
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg [
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Dilution Factor 10 1 QC Limits
Surrogate Recovery:
o-Terphenyl 91 100 30- 150 %
Quality Assurance / Quality Control Data
QC Reference No. 020413-BL
Analytes:
Diesel
LCS
% Rec.
86
LCS
QC Limits
80-120
Spike
% Rec.
84
Spike Dup.
% Rec.
80
Spike
QC Limits
50-150
RPD
4.9
RPD
QC Limits
0-30
ND means Not Detected
Reporting Limit (RL) = Practical Quantitation Limit (PQL) x Dilution Factor
HC = Hydrocarbon
• - Surrogate diluted out.
.qiFRRA ANALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA 92123
Sierra Project No.:
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213 Analyst:
104567002 3354 & 3366 Madison St., Carlsbad
Soil ' ' Report Date: /: 04/
2320
04/11/02
04/11/02
04/15/02
04/15/02
SM
.5/02
Volatile Organics (GC/MS)
Preparation Method: Purge & Trap Concentrator (EPA Method 5030)
Analysis Method: EPA Method 8260B
Client Sample No.
Sierra Sample No.:
SPl
7566
Practical
Quantitation
Limit
Units
Analytes:
Benzene ND
Bromobenzene ND
Brompchloromethane ND
Bromodichloromethane • \;ND ;..
Bromoform ND
Bromomethane ND
n-Butylbenzene ND
sec-Butylbenzene ND
tert-Butylbenzene ND
Carbon tetrachloride ND
Chlorobenzene ND
Chloroethane ND
Chloroform ND
Chloromethane ND
2-Chlorotoluene ND
4-Chlorotoluene ND
Dibromochloromethane ND
l,2-Dibromo-3-chloropropa ND
1,2-Dibromoethane ND
Dibromomethane ND
l^Dichlorobenzene ND
1,3-Dichlorobenzene ND
1,4-Dichlorobenzene ND
Dichlorodifluoromethane
1 l-Dichloroethane
ND
ND
5.0 ^ig/kg
5.0 (.ig/Tcg
5.0 (jg/T<g
5.0,; ; / l^g'kg,
5,0-. • Hg-'^g . ..
5.0 Hg/kg
5.0 ^g/Tcg
5.0 Hg/lcg
5.0 Pg/kg
5.0 [ig/kg
5.0 Hg/kg
5.0 Hg/kg
5.0 lig/kg
5.0 ^g/kg
5.0 Hg/kg
5.0 lig/kg
5.0 Hg/kg
5.0 ^ig/kg
5.0 Hg/kg
5.0 Mg/kg
5.0 Hg/kg
5.0 lig/Tcg
5.0 Hg/kg
5.0 ]ig/kg
5.0 Hg/kg
SIERRA ANALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA 92123
Sierra Project No.;
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared
Date Analyzed
0204-213 Analyst:
104567002 3354 & 3366 Madison St., Carlsbad
Soil . V ; Report Date: V . 04/15/02
2320
04/11/02
04/11/02
04/15/02
04/15/02
SM
Volatile Organics (GC/MS)
Preparation Method: Purge & Trap Concentrator (EPA Method 5030)
Analysis Method: EPA Method 8260B
Client Sample No.:
Sierra Sample No.:
SPl
7566
Analytes:
1,2-Dichloroethane ND
1,1-Dichloroethene ND
cis 1,2-Dichloroethene ND
trans 1,2-Dichloroethene ND
1,2-Dichloropropane • ND' 1,3-Dichloropropane ND
2,2-Dichloropropane ND
1,1-Dichloropropene ND
cis-l,3-Dichloropropene ND
trans-1,3-Dichloropropene ND
Ethylbenzene ND
Hexachlorobutadiene ND
Isopropylbenzene ND
4-Isopropyltoluene ND
Methylene Chloride ND
Methyl-t-Butyl ether (MTBE) ND
Napthalene ND
n-Propylbenzene ND
Styrene ND
1,1,1,2-Tetrachloroethane ND
1,1,2,2-Tetrachloroethane ND
Tetrachloroethene ND
Toluene ND
1.2.3-Trichlorobenzene ND
Practical
Quantitation
Limit
Units
5.0 Mg/kg
5.0 Hg/kg
5.0 Mg/kg
5.0 - • Mg/kg
5.0 • . , • Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
SIFRRA ANALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA 92123
Sierra Project No.:
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213 Analyst:
104567002 3354 & 3366 Madison St., Carlsbad
Soii^ ^ ^- . Report Date:; ; 04/15/02
2320
04/11/02
04/11/02
04/15/02
04/15/02
SM
Volatile Organics (GC/MS)
Preparation Method: Purge & Trap Concentrator (EPA Method 5030)
Analysis Method: EPA Method 8260B
Client Sample No.:
Sierra Sample No.:
SPl
7566
Practical
Quantitation
Limit
Units
Analytes:
1.2.4- Trichlorobenzene
1,1,1-Trichloroethane
,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
,2,4-Trimethylbenzene
1.3.5- Trimethylbenzene
Vinyl Chloride
m,p-Xylenes
o-Xylene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.0.
5:0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
Mg/kg
Mg/kg
Mg/kg
Mg/kg
i-ig/kg.
Mg/kg
Mg/kg
Mg/kg
Mg/kg
Mg/kg
Mg/kg
QC Reference INo.:
Analytes:
LCS
% Rec.
LCS
QC Limits
Spike
%Rec.
Spike Dup.
% Rec.
Spike
OC Limits RPD RPD
QC Limits
1,1-Dichloroethene
Trichloroethene
Benzene
Toluene
Chlorobenzene
94
90
92
90
88
80 - 120
80- 120
80- 120
80 - 120
80 - 120
110
102
102
100
98
100
96
96
94
94
50- 150
71 - 157
37-151
47- 150
37 - 160
• 9.5
6.1
6.1
6.2
4.2
0 - 30
0-30
0-30
0-30
0-30
ND means Not Detected
Reporting Limit (RL) = Practical Quantitation Limit (PQL) x Dilution Factor
SIERRA ANALYTICAL
Ninyo and Moore
5710 Ruffin Road, Suite #B204
San Diego, CA 92123
Sierra Project No.
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213 : , .. Analyst:: ;
104567002 3354 & 3366 Madison St., Carlsbad
Soil Report Date:
2320
04/11/02
04/11/02
04/15/02
04/16/02
JBN/BW
04/17/02
CCR Title 22 Metals (TTLC)
Preparation Method: EPA Method 3050B
Analysis Method: EPA Method 6010B & EPA Method 7471*
Client Sample No.: SP 1 Practical
Quantitation
Limit
Units
Sierra Sample No.: 7566
Practical
Quantitation
Limit
Units
Analytes: TTLC Limits:
Antimony 500 ND 3.85 mg/kg
Arsenic 500, ' . , • • ND • • : 2.00 • mg/kg
Barium 10000 " '- 57.1^ • ; /; 2.00^ ^ • mg/kg..
Beryllium 75 ND 075 mg/kg
Cadmium 100 ND 0.50 mg/kg
Chromium 2500 16.0 2.00 mg/kg
Cobalt 8000 5.67 2.00 mg/kg
Copper 2500 5.92 2.50 mg/kg
Lead 1000 37.2 2.00 mg/kg
Mercury* 20 0.032 0.030 mg/kg
Molybdenum 3500 ND 1.50 mg/kg
Nickel 2000 7.70 1.00 mg/kg
Selenium 100 ND 1.52 mg/kg
Silver 500 ND 1.00 nig/kg
Thallium 700 ND 2.00 mg/kg
Vanadium 2400 45.6 1.00 mg/kg
Zinc 5000 99.6 2.00 mg/kg
Dilution Factor -~
ND means Not Detected
Reporting Limit = Practical Quantitation Limit x Dilution Factor
Results reported on an "As Is" basis, not dry weight.
SIERRA ASJALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA. 92123
Sierra Project No.
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213 Analyst:
104567002 / 3354 & 3366 Madison St, Carlsbad
Soil ReportDate: 04/17/02
2320
04/11/02
04/11/02
04/12/02
04/12-04/17/02
RF
Client Sample No.
Sierra Sample No.
SP 1
7566
Method No. Detection
Limit
TEST PARAMETERS UNITS
pH Units 6.1 EPA 9045 0,1
Dilution Factor
ND means Not Detected
Reporting Limit = (Practical Quantitation Limit x Dilution Factor)
.qiFRRA ANALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA 92123
Sierra Project No.:
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213-Addendum Analyst:
104567002 3354 & 3366 Madison St., Carlsbad
Soil : Report Date:, 04/23/02
2320
04/11/02
04/11/02
04/22/02
04/22/02
SM
Volatile Organics (GC/MS)
Preparation Method: Purge & Trap Concentrator (EPA Method 5030)
Analysis Method: EPA Method 8260B
Client Sample No.;
Sierra Sample No.:
SSW-02
7562
Practical
Quantitation
Limit
Units
Analytes:
Benzene ND
Bromobenzene ND
Bromochloromethane ND
Bromodichloromethane ' " : ' • ND: ;
Bromoform - ND
Bromomethane ND
n-Butylbenzene ND
sec-Butylbenzene ND
tert-Butylbenzene ND
Carbon tetrachloride ND
Chlorobenzene ND
Chloroethane ND
Chloroform ND
Chloromethane ND
2-Chlorotoluene ND
4-Chlorotoluene ND
Dibromochloromethane ND
1,2-Dibromo-3-chloropropa ND
1,2-Dibromoethane ND
Dibromomethane ND
1,2-Dichlorobenzene ND
1,3-Dichlorobenzene ND
1,4-Dichlorobenzene ND
Dichlorodifluoromethane ND
1 l-Dichloroethane ND
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 :; Mg/kg-
5-0. y. • Mg/kg.
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
.'SIERRA ANALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA 92123
Sierra Project No.:
Client Project ID:
Sample Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213-Addendum Analyst:
104567002 3354 & 3366 Madison St„ Carlsbad
Soil ReportDate: • 04/23/02
2320
04/11/02
04/11/02
04/22/02
04/22/02
SM
Volatile Organics (GC/MS)
Preparation Method: Purge & Trap Concentrator (EPA Method 5030)
Analysis Method: EPA Method 8260B
Client Sample No.;
Sierra Sample No.:
SSW-02
7562
Practical
Quantitation
Limit
Units
Analytes:
1,2-Dichloroethane ND
1,1-Dichloroethene ND
cis 1,2-Dichloroethene ND
trans i ,2-Dichloroethene : , ND..
1,2-Dichloropropane 'ND-
1,3-Dichloropropane ND
2,2-Dichloropropane ND
1,1-Dichloropropene ND
cis-1,3-Dichloropropene ND
trans-1,3-Dichloropropene ND
Ethylbenzene ND
Hexachlorobutadiene ND
Isopropylbenzene ND
4-Isopropyltoluene ND
Methylene Chloride ND
Methyl-t-Butyl ether (MTBE) ND
Napthalene ND
n-Propylbenzene ND
Styrene ND
1,1,1,2-Tetrachloroethane ND
1,1,2,2-Tetrachloroethane ND
Tetrachloroethene ND
Toluene
1,2,3-Trichlorobenzene
ND
ND
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0--; . . 'Mg/kg
5.0 .; Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
5.0 Mg/kg
SIERRA ANALYTICAL
Ninyo & Moore
5710 Ruffin Road
San Diego, CA 92123
Sierra Project No.:
Client Project ID:
Sample; Matrix:
ELAP No.:
Date Sampled:
Date Received:
Date Prepared:
Date Analyzed:
0204-213-Addendum Analyst:
104567002 3354 & 3366 Madisori St., Carlsbad
Soil : ' Report Date: ; . 04/23/02
2320
04/11/02
04/11/02
04/22/02
04/22/02
SM
Volatile Organics (GC/MS)
Preparation Method: Purge & Trap Concentrator (EPA Method 5030)
Analysis Method: EPA Method 8260B
Client Sample No.;
Sierra Sample No.;
SSW-02
7562
Practical
Quantitation
Limit
Units
Analytes:
1,2,4-Trichlorobenzene ND
1,1,1-Trichloroethane ND
l,I,2TTrichloroethane ND
Trichloroethene .• •:;ND.
trichlorofluoromethane ND-
1,2,3-Trichloropropane ND
1,2,4-Trimethylbenzene ND
1,3,5-Trimethylbenzene ND
Vinyl Chloride ND
m,p-Xylenes ND
o-Xylene ND
Dilution Factor 1
Surrogate Recovery:
105 Dibromofluoromethane 105
Toluene-d8 99
4-Bromofluorobenzene 102
5.0
5.0
5.0
5:0'
is.6.
5.0
5.0
5.0
5.0
5.0
5.0
Mg''kg
Mg'kg
Mg''kg
Mg/kg
Mg/kg;
Mg/kg
Mg'kg
Mg/kg
Mg/kg
Mg/kg
Mg''kg
QC Limits
80- 120
81- 117
74-121
%
Quality Assurance / Quality Control Data
QC Reference No.: 020422-7928
Analytes: LCS
% Rec.
LCS
OC Limits
Spike
% Rec.
Spike Dup.
% Rec.
Spike
QC Limits RPD RPD
QC Limits
1,1-Dicliloroethene
Trichloroethene
Benzene
Toluene
Chlorobenzene
92
92
90
92
90
80 - 120
80 - 120
80- 120
80-120
80-120
94
92
90
90
90
94
88
90
88
88
50-150
71 - 157
37 - 151
47 - 150
37 - 160
0.0
44
0.0
2.2
2.2
0 - 30
0-30
0 - 30
0-30
0-30
ND means Not Detected
Reporting Limit (RL) = Practical Quantitation Limit (PQL) x Dilution Factor
SIERRA ANALYTICAL
Ninyo and Moore ELAP No.: 2320
5710 Ruffin Road Date Sampled: 04/11/02
San Diego, CA 92123 Date Received: 04/11/02
Date Prepared: 04/24/02
Date Aiialyzed: 04/25/02,. -
Sierra Project No.: 0204-213-Addendum Analyst: -...JBN/BW/..:.;
Client Project ID: 104567002 / 3354&3366 Madison St., Carlsbad
Sample Matrix: Soil Report Date: 04/26/02
CCR Title 22 Metals (TTLC)
Preparation Method: EPA Method 3050B
Analysis Method: EPA Method 6010B & EPA Method 7471*
Client Sample No.: SSW-02 Practical
Quantitation
Limit
Units
Sierra Sample No.: 7562
Practical
Quantitation
Limit
Units
Analytes: TTLC Limits:
Antimony 500 ND 3.85 mg/kg
Arsenic. . ... ;. 500' A: • ND •:. 2.-00 . .mg/kg •
Barium loboo 12.0 2.00-mg/kg
Berylliiun 75 ND 0.75 • mg/kg
Cadmiimi 100 ND 0.50 mg/kg
Chromium 2500 11.3 2.00 mg/kg
Cobalt 8000 2.85 2.00 mg/kg
Copper 2500 5.92 2.50 mg/kg
Lead 1000 15.0 2.00 mg/kg
Mercury* 20 ND 0.030 mg/kg
Molybdenum 3500 ND 1.50 mg/kg
Nickel 2000 3.91 1.00 mg/kg
Selenium 100 ND 1.52 mg/kg
Silver 500 ND 1.00 mg/kg.
Thallium 700 ND 2.00 mg/kg
Vanadiiun 2400 33.9 1.00 mg/kg
Zinc 5000 33.3 2.00 mg/kg
Dilution Factor ---
ND means Not Detected
Reporting Limit = Practical Quantitation Limit x Dilution Factor
Results reported on an "As Is" basis, not dry weight.
Sierra Project Number
Client Name:
Client Project ID ::
Project Addendum / Change Order
0204-213 Sierra Project manager: Suzanne / Justin
Ninyo & Moore Turn Around Time : Normal
104567002 . Sample Location: B-2
Sierra
7562 Soil Analyze for EPA 8260 / Title 22 Metals
Addendum / Change Order Taken By
Signature
04/22/02 9:30
Date Time
Addendum / Change Order Requested By;
Travis Stravasnik
Printed Name
Requested Via:
FAX Letter (Phone) In Person
Sierra Project Number;
Client Name:
Client Project ID :
Project Addendum / Change Order
0204-213
Ninyo & Moore
104567002
Sierra Project manager: Andrew
Turn Around Time : Normal
Sample Location : B-2
Sierra
7562 Soil Report as CCID
7564 Soil Report as CCID
Addendum / Change Order Taken By :
A-rvd/mv- Xum
Signature
04/30/02 13:30
Date Time
Addendum / Change Order Requested By:
Travis Stravasnik
Printed Name
Requested Via:
FAX Letter ( Phone) In Person
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